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Date Work Order <br /> 30-May-01 Alpha Analytical, Inc - QC Summary Report 01051893 <br /> Method Blank Type MBLK Test Code SW8015 Batch ID MS12W0521D <br /> File ID D 1MSDCHEMIMSI2�DATA1010524101052430 D Analysis Date 05/24/2001 20 10 <br /> Sample ID MBLK MS12W0524A Units mg1L Run ID GCIMSD_12_010521 B Prep Date 05124/2001 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPD Ref Val %RPD Qual <br /> TPH Purgeable ND 005 <br /> Surr 1,2-D)Chloroethane-d4 000991 001 99 70 13D <br /> Surr Toluene-d8 000963 001 96 70 130 <br /> Surr 4-Bromofluorobenzene 000886 001 89 70 130 <br /> Laboratory Control Spike Type LCS Test Code SW8015 Batch ID MS12W0521D <br /> File ID D 1MSDCHEM1MS121DATA1010524101052425 D Analysis Date 05124/2001 18 25 <br /> Sample ID GLCS MS12W0521C Units mg1L Run iD GCIMSD_12_010521B Prep Date 05124/2001 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPD Ref Val %RPD Qual <br /> TPH Purgeable 0 382 005 D 4 95 56 136 <br /> Surr 1 2-Dichloroethane d4 00106 001 106 70 130 <br /> Surr Toluene-d8 000922 001 92 70 130 <br /> Surr 4-Bromofluorobenzene 00101 001 101 70 130 <br /> Sample Matrix Spike Type MS Test Code SW8015 Batch ID MS12W0521D <br /> File ID D 1MSDCHEMIMS12tiDATA1010524101052428 D Anaiys:s Date 05/24/2001 19 28 <br /> Sample ID 01051893-01AGS Units mglL Run ID GCIMSD_12-0105218 Prep Date 05/2412001 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit H:ghLimit RPD Ref Val %RPD Qual <br /> TPH Purgeable 204 0 25 2 0 102 56 136 <br /> Surr 1 2-Dichloroethane-d4 00478 005 96 70 130 <br /> Surr Toluene-d8 00468 005 94 70 130 <br /> Surr 4-Bromofluorobenzene D 0486 005 97 7D 130 <br /> Sample Matrix Spike Duplicate Type MSD Test Code SW8015 Batch ID MS12W0521D <br /> File iD D 1MSDCHEMIMSI2LDATA1010524101052429 D Analysis Date 05/2412001 19 49 <br /> Sample ID 01051693-01AGSD Units mglL Run ID GC/MSD_12 0105216 Prep Date 05/24/2001 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPD Ref Val %RPD Qual <br /> TPH Purgeable 1 99 025 2 0 99 56 136 2042 284 <br /> Surr 1 2-Dichloroethane-d4 00497 005 99 70 130 <br /> Surr 7oluene-d8 00477 005 95 70 130 <br /> Surr 4-Bromofluorobenzene 00496 005 99 70 130 <br /> Commc.uts ND Not Detected at the Reporting Limit D-If the spiked value is<25%of the reference value,recovery should not be calculated <br /> S-Spike Recovery outside accepted recovery limits M-Spike Recovery outside accepted recovery limits due to matrix <br /> B-Arialyte detected in the associated Method Blank <br /> • <br />