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Date ��ork Order ra,sc,�oo Alpha Analytical, Inc - C Summary Report 00090560 Method$lank Test Code SW8260B Batch ID MS8WO906A Analysis Date 09/0612000 13 05 Sample ID MBLK MS8WO906AIB Units pgJL Run ID GCIMSD_8_000906APrep Date 09/06/2000 Analyte Result PQL SpkVal SpkRefVal %REC LowLimtt Hight-imtt RPD Ref Val %RPD Qual erttary Butyl Alcohol(TBA) ND 10 ethyl tert-butyl ether(MTBE) NO 0 5 Di-isopropyl Ether(DEPS) NO 1 Ethyl Tertiary Butyl Ether(ETRE) NO 1 Benzene ND 0 5 Tertiary Amyl Methyl Ether(TAME) ND 1 Toluene ND 0 5 Ethylbenzene ND 0 5 m,p-Xylene ND 0 5 o-Xylene ND 0 5 Surr 1,2-Dtchloroethane-d4 109 10 109 68 139 Surr Toluene-d8 101 10 101 75 127 Surr 4-Bromofluorobenzene 106 10 106 73 128 Laboratory Control Spike Test Code SW8260B Batch ID MS8WO906A Analysis Date 09/07/2000 10 33 Sample ID LCS MS8WO906A Units pg/L Run ID GC/MSD_8_000906APrep Date 09/07/2000 Analyte Result PQL SpkVal SpkRefVal %REC LowLimlt Hight-imit RPD Ref Val %RPD Qual Methyl tent-butyl ether(MTBE) 107 0 5 10 107 '0 142 Benzene 969 0 5 10 97 76 127 Toluene 9 7 0 5 10 97 76 125 Ethylbenzene 102 0 5 10 102 64 132 m,p-Xylene 206 0 5 20 103 70 130 o-Xylene 103 0 5 10 103 70 130 Surr 1,2-Dtchloroethane-d4 109 10 109 68 139 Surr Toluene-d8 101 10 101 75 127 Surr 4-Bromofluorobenzene 107 10 107 73 128 Sample Matrix Spike Test Code SW8260B Batch ID MS8WO906A Analysis Date 09/07/2000 08 49 Sample ID 00090560-OIAMS Units Vg/L. Run 1D GCIMSD_8_000906APrep Date 09/07/2000 Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLtmtt RPD Ref Val %RPD Qua] Methyl tent-butyl ether(MTBE) 52 8 2 5 50 0 106 70 142 WEllenzene 526 2 5 50 0 105 76 127 oluene 51 4 2 5 50 0 103 76 125 Ethylbenzene 54 6 2 5 50 0 109 64 132 m p-Xylene 110 2 5 100 0 110 70 130 o-Xylene 54 4 2 5 50 0 109 70 130 Surr 1,2-Dtchloroethane-d4 586 50 117 68 139 Surr Toluene-d8 495 50 99 75 127 Surr 4-Bromofluorobenzene 54 1 50 108 73 128 Sample Matrix Spike Duplicate Test Code SW8260B Batch ID MSBW0906A Analysts Date 09/07/2000 09 15 Sample lD 00090560-OIAMSD Units pg/L Run ID GC/MSD_8_000906APrep Date 09/0712000 Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPD Ref Val %RPD Qua[ Methyl tert-butyl ether(MTBE) 53 6 2 5 50 0 107 70 142 5276 1 56 , Benzene 52 6 2 5 50 0 105 76 127 52 55 0 114 Toluene 507 2 5 50 0 101 76 125 51 38 1 23 Ethylbenzene 543 2 5 50 0 109 64 132 54 59 0 533 m,p-Xylene 110 2 5 100 0 110 70 130 1098 00273 o-Xylene 54 3 2 5 50 0 109 70 130 5443 0 165 Surr 1 2-Dichloroethane-d4 58 5 50 117 68 139 Surr Toluene-d8 49 4 50 99 75 127 Surr 4-Bromofluorobenzene 53 50 106 73 128 omments ND-Not Detected at the Reporting Limit D-If the spiked value is<25%of the reference value,recovery should not be calculated S-Spike Recovery outside accepted recovery limits M-Spike Recovery outside accepted recovery limits due to matrix B- Analwe detected in the associated Method Blank