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Laboratories Inc. <br /> Environmental Testing Laboratory Since 1949 <br /> Stantec Reported: 03129/2011 9:49 <br /> 3475 W.Shaw Avenue,Suite 104 Project: Calpines <br /> Fresno,CA 93711 Project Number. 185802343 <br /> Project Manager: Ralph Carson <br /> Base Neutral and Acid Extractables Organic Analysis (EPA Method 8270C) <br /> Quality Control Report - Precision & Accuracy <br /> Control Limits <br /> Source Source Spike Percent Percent Lab <br /> Constituent Type Sample ID Result Result Added Units RPD Recovery RPD Recovery Quals <br /> QC Batch ID: BUC1852 Used client sample. N <br /> 2-Methylphenol MS 110411502 NO 1.5117 1.6892 mg/kg 89.5 39-116 <br /> MSD 110411502 NO 1.4939 1.6722 mg/kg 1.2 89.3 25 39-116 <br /> 3-&4-Methylphenol MS 1104115-02 NO 2.2166 3.3784 mg/kg 65.8 40-102 <br /> MSD 1104115-02 NO 2.1850 3.3445 mg/kg 1.4 65.3 24 40-102 <br /> 4-Nitrophenol MS 1104115-02 NO 1.7334 1.6892 mg/kg 103 32-111 <br /> MSD 110411502 NO 1.8587 1.6722 mg/kg 7.0 111 17 32-111 <br /> Pentachlorophenol MS 1104115-02 NO 1.2836 1.6892 mg/kg 76.0 20-134 <br /> MSD 1104115-02 NO 1.2426 1.6722 mg/kg 3.2 74.3 25 20-134 <br /> Phenol MS 110411502 NO 1.0375 1.6892 mg/kg 61.4 38-113 <br /> MSD 1104115-02 NO 1.0259 1.6722 mg/kg 1.1 61.3 25 38-113 <br /> 2,4,6-Tnchbtophenol MS 1104115-02 NO 1.4345 1.6892 mg/kg 84.9 58-119 <br /> MSD 110411502 NO 14090 1.6722 mg/kg 1.8 84.3 24 58-119 <br /> 2-Fluorophenol(Surrogate) MS 110411502 NO 2.2941 2.7027 mglkg 84.9 25-144 <br /> MSD 1104115-02 NO 2.3044 2.6756 mg/kg 0.5 86.1 25-144 <br /> Phenol-:15(Surrogate) MS 1104115-02 NO 1.9831 2.7027 mpg 73.4 26-133 <br /> MSD 110411502 NO 1.9896 2.6756 mg1kg 0.3 74.4 26-133 <br /> Nitrobenzene-d5(Surrogate) MS 110411502 NO 2.3799 2.7027 mgfkg 88.1 39-113 <br /> MSD 110411502 NO 2.3195 2.6756 m9/kg 2.6 86.7 39-113 <br /> 2-Fluorobiphenyl(Surrogate) MS 1104115-02 NO 1.7242 2.7027 mg/kg 63.8 43-120 <br /> MSD 110411502 NO 1.6333 2.6756 mg/kg 5.4 61.0 43-120 <br /> 2,4,6-Tribromophenol(Surrogate) MS 1104115-02 NO 3.1193 2.7027 mg/kg 115 31-147 <br /> MSD 110411502 NO 3.1939 2.6756 mg/kg 2.4 119 31-147 <br /> p-Terphenyl-d14(Surrogate) MS 110411502 NO 1.0457 1.3514 mg/kg 77.4 37-149 <br /> MSD 110411502 NO 0.98475 1.3378 mg/kg 8.0 73.6 37-149 <br /> %he r su/tr m this rcparr apply m rhe samples analyzed in accordance wish Ne chain ujcusrsaAy d«vment%hia unufylicol rcpnrr matin Ae repruAucrd in us emirrry. <br /> All r®alts IisW in this repo/are for the endusive use ofthe suMnininy parry. BC lebomtories,IM.assumes no r«pomibiliry fw repo/altension,separation,deuchmem or third pant imerpretation. <br /> 4100 Atlas Court Bakersfield,CA 93308 (861)327-4911 FAX(661)327-1918 www.bdabs.com Page 42 of 54 <br />