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110 2nd.Avenue South,#D7,Pacheco. CA 94153-5j6J <br /> 4 MCCANITBELL AtiALYTICAL INC. Telephone� 925-798-1620 Fax . 925-798-M-72 <br /> http://Www.mccampbell.com E-mail: main(&rrocampbell.com <br /> - Advanced Geo%nvironmentalI Client Project ID: Municipal Service Date Sampled: 02/04/02 <br /> 837 Shaw Road Center Date Received: 02/05/02 <br /> Stockton. CA 95215 Client Contact: Brian Millman Date Extracted: 02/08-02/11/02 <br /> Client P.O: Date Analyzed: 02/08-02,11/02 <br /> Volatile Organics By GC/MS <br /> EPA method 3260 <br /> Lab ID 89608 <br /> Client ID SB-H,0 <br /> Matrix W <br /> Repuning Limii Repurting Lima <br /> Compound Concentration* - Compound Concentration* <br /> �=W E � I -W I 5 <br /> Acetonei61 ND 5.0 25 trans-t,3-Dichloropropene ND 1.0 /.O <br /> Benzene ND 1.0 5.0 Ethylene dibromide ND 1.05.0 <br /> Bromobenzene ND 1.0 ! 5.0 Ethyibenzene ND j 1.0 5.0 <br /> Bromochloromethane ND LO I 5.0 ,iexachlorobutadiene ND 5.0 25 <br /> Bromodichloromethane ND 1.0 7 5.0 lodomethane ND 1.0 j no <br /> Bromotorm ! ND 1.0 5.0 lsopropylbenzene ND 1.0 5.0 <br /> Bromomethane j ND .0 5.0 p-Isopropyl toluene ND ].O 5.0 <br /> n-Butyl benzene ND 1.0 5,0 Methyl butyi ketone' ND 1.0 5.0 <br /> j sec-Butyl benzene ND 1.0 5.0 Methylene Chloride`" ND I.0 5.0 <br /> tert-Butyl benzene ND ].0 5.0 Methyl ethyl ketone' ND ?.0 U <br /> r - <br /> Carbon Disulfide ND 1.0 S.D Methyl isobutyl ketone's' I ND LO 5.0 <br /> Carbon Tetrachloride ND 1.0 5.0 Methyl tert-Butyl Ether(MTBE) I --moi LO S.0 <br /> " Chiorobenzene ND 1.0 5.0 Naphthalene ND 5.0 25 <br /> Chloroethane ND I ()-1 5.0 n-Propyl benzene ND 1.0 5-0 j <br /> 2-Chloroethyl VinVI Ether'" ND l.o 5.0 Styrene` ND 1.0 0 <br /> Chlorotorm 2.0 1 1.0 5.0 I 1,I,12-Tetrachloroethane j ND 1.0 5.0 <br /> ' Chloromethane ND I 1.0 5.0 1,1,2,2-Tetrachloroethane ND I.0 sit0o <br /> 2-Chlorotoluene ND 1.0 5.0 Tetrachloroethene <br /> 4-Chlorotoluene ND 1.0 5.0 Toluene' ND i.0 q <br /> Dibromochloromethane ND 1.0 5.0 1,2,3-Trichlorobenzene ND 5.0 25 1 <br /> 1,2-Dibromo-3-chtoropropane ND 2.0 10 1,2,4-Trichlorobenzene I ND 5.0 25 <br /> Dibromomethane ND LO 5.0 1,1,1-Trichloroethane ND 1.0 5.0 <br /> 1,2-Dichlorobenzene ND 1.0 j 5.0 1,1,2-Trichloroethane ND LO J 5.0 <br /> I,3-Dichlorobenzene ND 1.0 5.0 Trichloroethene ND 1.0 5.0 <br /> 1,4-Dichlorobenzene ND LO S.0 'Trichlorofluoromethane ND 1.0 Llm0 <br /> Dichlorodifluoromethane ND 1.0 5.0 1,2,3-Trichloropropane ND LO 5.(1 <br /> 1,1-Dichloroethane ND l.O 5.0 1,2,4-Trimethyibenzene ND 1.0 5.0 <br /> 1,2-Dichloroethane ND LO 5.0 1,3,5=rrimethylbenzene ND 1.0 S_0 <br /> 1,:-Dichloroethene ND 1.0 5.0 ! Vinyl Acetate""' ND 5.0 25 <br /> cis-1,2-Dichloroethene ND 1.0 5.0 Vinyl Chloride'"' ND LO ; 5.0 <br /> trans-1,2-Dichloroethene ND 1.0 5.0 Xylenes,total '0 ND Llo 5.0 j <br /> ,2-Dichloropropane ND LO 5.0 Comments: i <br /> 1,3-Dichloropropane ND 1.0 5.0 Surrogate Recoveries(%) <br /> 2?-Dichloropropane ND 1.0 5.0 DibromOtInOrOmethane 105 <br /> I,1-Dichloropropene ND LO 5.0 Toluene-d8 103 <br /> cis-1,3-Dichloropropene ND LO 5.0 4-Bromotluorobenzene 100 <br /> water and vapor samples are reported in❑g/L,soil and sludge samples in ug/kg,wipes in ughvipe and all TCLP/SPLP extracts in ug/T. <br /> ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene; (d) 2-hexanone; (e) dichloromethane; (0 2-butanane; (g) 4-methyl-?- <br /> i pentanone or isopropyiacetone; (h) lighter than water immiscible sheen is present; (i)liquid sample that contains greater than --5 vol. °;, <br /> sediment; 0) sample diluted due to high organic content; Ik) ethenylbenzene; (1) methylbenzene; (m) acetic acid ethenyl ester; (n) <br /> chloroethene;(o)dime thy]benzenes. <br /> DHS Certification No. 1644 Edward Hamilton, Lab Director <br />