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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> t 4MCCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax:925-798-1622 <br /> hh j://www.mccam�ell.cp E-mail:main@mccampbell.com <br /> Advanced GeoEnvirorimental Client Project ID:Cole Date Sampled: 08/23-08/24/99 <br /> ' 4005 North Wilson Way Date Received: 08/25/99 <br /> Stockton, CA 95205 Client Contact: Bill Little Date Extracted: 08/25/99 <br /> ' Client P.O: Date Analyzed: 08/26/99 <br /> EPA method 8260 modified <br /> Oxygenated Volatile Organics By GC/MS <br /> ' Lab ID 17932 17933 17934 17935 <br /> Reporting Limit <br /> Client ID MW1/8-24-99 MWt-15 MW140 MW1-50 <br /> ' Matrix W S S S S W <br /> Compound Concentration* ug/kg ug/L <br /> Di-isopropyl Ether(D1PE) ND<3.5 ND ND N < <br /> D ]0 _ 5.0 ].0 <br /> ' Ethyl tert-Butyl Ether(ETBE) ND<3.5 ND ND ND<10 5.0 1.0 <br /> ' Methyl-tert Butyl Ether(MTBE) 97 ND ND 180 5.0 1.0 <br /> tert-Amyl Methyl Ether(TAME) ND<3.5 ND ND ND<10 5.0 1.0 <br /> tert-Butanol ND<18 ND ND ND<50 25 5.0 <br /> Surrogate Recoveries(%) <br /> Dibromofluoromethane 95 94 93 107 <br />' Comments: <br /> *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/Mpe and all TCLP 1 STLC 1 SPLP extracts in ug/L <br />' ND means not detected above the reporting limit;NIA means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present; (i)liquid sample that contains greater than—5 vol. /a sediment;0)sample diluted due to <br /> high organic content <br />' DHS Certification No. 1644 1 40 Edward Hamilton,Lab Director <br /> 1 <br />