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N <br /> f <br /> GeoAnalytical Laboratories , Inc.. <br /> 2300 Maryann Dr. Turlock, CA 95380 Phone (209) 669-0100 Fax (209) 593-2212 <br /> email : lah.geo@atr.net <br /> Report # Y2K1601 Date: 11 /27/ 12 <br /> Jim Thorpe, Inc. Date Recd : 11 / 16/12 <br /> P.O Box 357 <br /> Lodi, CA 95241 <br /> Volatile. Organic Chemistry - Quality Control <br /> GeoAnalytical Laboratories, Inc. <br /> Reporting Spike Source %REC RPD <br /> Anal le Result Limit Units Level Result /REC Limits RPD Limit Notes <br /> Batch Y003100 - EPA 5030 Prepared & Analyzed: 11/26/12 <br /> Blank (Y003100-BLKI ) - <br /> Benzene ND 5.0 ug/kg <br /> Di-isopropyl Ether (DIPE) ND 10.0 it <br /> Ethanol ND 400 it <br /> Ethyl tert-Butyl Ether (ETBE) ND 10.0 IF <br /> Ethylbenzene ND 5.0 <br /> Methyl tert-Butyl Ether (MTBE) ND 10.0 " <br /> Tert-Amyl Methyl Ether (TAME) ND 10.0 It <br /> tert-Butanol (TBA) ND 200 " <br /> Toluene ND 5,0 It <br /> Xylenes, total ND 5.0 It <br /> Gasoline ND 1 .0 mg/kg <br /> Surrogate: 1,2-Diehloroethane-d4 19, 6 ng/kg 20. 00 98 72-132 <br /> Surrogate: 2-Brorua-1-Chloropropane 16.5 If 20.00 83 71-134 <br /> Surrogate: 4-Bromoj1mrobeecene 19.3 IF20. 00 97 74-132 <br /> Surrogate: 1,2-Dichloroerhane-d4 0.0196 mglkg 0.02000 98 72-132 <br /> Surrogate: 2-Bromo-1-Chloropropane 0.0165 If0. 02000 83 71-134 <br /> .Surrogate: 4-Bromojhtoroben_ene 0. 0193 It 0. 02000 97 74- 132 <br /> LCS (Y003100-BSI) _ -- _ _ <br /> Benzene 55.2 5.0 ug/kg. 6000 92 80- 120 <br /> Di-isopropyl Ether (DIPE) 51 .6 10.0 " 60.00 86 80-120 <br /> Methyl lert-Butyl Ether (MTBE) 57.5 10.0 It 60.00 96 80-120 <br /> Tert-Amyl Methyl Ether (TAME) 56.5 10.0 " 60.00 94 80-120 <br /> Toluene 57,6 5.0 160,00 96 80-120 <br /> Gasoline 1 .2 1-0 mg/kg 1 .500 81 80- 120 <br /> Surrogate: 1,2-Dich1oroerhane-d4 19.9 ug/kg 20v6O 100 72-132 <br /> Surrogare: 2-Bromo-1-Chloropropane / 7- 0 If20.00 85 71-134 <br /> Surrogate: 4-Bram jluorobencene 18.4 It20.00 92 74-131 <br /> Surrogate: 1,2-Dichloroethane-d4 0.0198 mg/kg 0.02000 99 72-132 <br /> Surrogate: 2-Bromo- l-Chloropropane 0,0166 " 0. 02000 83 71-134 <br /> Surrogate: 4-BromoJhrorobence17e 0.. 0193 It0. 02000 97 74- 132 <br /> Certification # 2585 <br />