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fi e <br /> Q11fluanterra <br /> 4r Environmental <br /> Services <br /> 4TRIX SPIKE/MATRIX SPIKE DUPLICATE QC REPORT <br /> etals Analysis and Preparation <br /> [Project: 092398 <br /> Lategory: ICP-S ICP'!Metals-Ottawa Sand LCS <br /> Test : ICP-CAMT-LO-S Method: 6010 <br /> Matrix : SOIL <br /> Uample : 092398-0010 <br /> Run : 31 MAR 97-M ' <br /> Units - : mg/kg Units QualifierY Wet wt. <br /> -=-------Concentration------ =- <br /> Amount Acceptance <br /> Sample MS MSD Spiked %Recovery %RPD Limit <br /> �Analyte Result Result Result MS MSD MS MSD Recov. !RPD <br /> ntimony ND 40:2 41.9 50.0 50.0 '80 84 4.2 80-120 50 <br /> Rarium 44!2 237 = 238 200 200 96 97 0.58 80-120 50 <br /> ND 4.72 <br /> Lryllium4.83 'y 5.00 5.00 94 97 2.3 80-120 50 <br /> dmium ND . 4.69 5.09 `" 5.00 5.00 94 102 8.2 80-120 50 <br /> Chromium 4.'3 22.3 23.5 20.0 20.0 90 96 5.2 80-120 50 <br /> ,)balt 3.''4 49.7 50.3 `" 50.0 50.0 93 94 1 .3 80-120 50 <br /> L`uer 13.8 37.4 41.5 25.0 25.0 94 111 10 80-120 50 <br /> bdenum ND 94.5 97.1 100 100 94 97 2.7 80-120 50 <br /> Nickel 6.3 50.5 51.5 J, 50.0 50.0 89 91 .2.0 80-120 50 <br /> � Iver ND 4.39 4.55 5.00 5.00 88 91 3.6 80-120 50 <br /> inadium 19.3 63.5 64.0 50:0 50.0 88 89 0.83 80-120 50 <br /> n 25.9 71 . 1 73.0 50.0 50.0 90 94 2.7 80-120 50 <br /> Category: GFAA10-S Furnace AA Metals <br /> Ltrixst : AS-QC-FAA-CAMT-S Method: 7060 <br /> : SOLID Ilk <br /> Sample : 092398-0001 <br /> " Run : 29 MAR 97-GA , } <br /> Ldits : mg/kg Units QualifierY Wet wt. <br /> ---------Concentration--------- <br /> Amount Acceptance <br /> L Sample MS MSD Spiked %Recovery%RPD Limit <br /> Analyte Result Result Result MS MSD MS MSD Recov. RPD <br /> Lt0 <br /> senic .877 4.03 4.04 4.00 4.00 79 79 0.25 75-125 20 <br /> dmium ND 0.206 0.200 0.200 0.200 103 100 3.0 75-125 20 <br /> Chromium 8.94 9.21 10.6 2.00 2.00 NC NC NC 75-125 20 <br /> lead . 1.76 3.62 3.85 2.00 2.00 93 104 6.2 75-125 20 <br />_ lenium ND 1.48 1.58 2.00 2.00 74 79 6.5 75-125 20 <br /> L!allium <br /> ND 4.78 4.69 5.00 5.00 96 94 1.9 75-125 20 <br /> NC = Not Calculated, calculation not applicable'. ., <br /> c = Not Detected <br /> alculations are performed before rounding to avoid round-off errors in calculated results. <br />