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Castle Analytical Laboratory,Atwater, CA <br /> Lab Report No H3082101 Date 08/29/2003 Page 2 <br /> ' Protect Name SUPER STOP MARKET Analysis Volatile Organic Compounds by GC/MS Fuel <br /> Protect No 6622 Method 8260FA <br /> Prep Meth SW5030B <br /> Field ID MW-104 Lab Samp ID 6003-4W <br /> Descr/Location MW-104 Recd Date 08/21/2003 <br /> Sample Date 08/20/2003 Prep Date 08/28/2003 <br /> Sample Time 0945 Analysis Date 08/28/2003 <br /> Matrix Water QC Batch VWMS-8283 <br /> Basis Not Filtered Notes <br /> ' Analyte Det Limit Rep Limit Note Result Units PvcDil <br /> Methyl-tert-butyl ether(MTBE) 0289 05 MRL 3.3 UGIL 1 <br /> ' Ethyl tent-butyl ether(ETRE) 0084 05 MRL ND UGIL 1 <br /> tert-Amyl methyl ether(TAME) 0 067 05 MRL ND UG/L 1 <br /> Di-isopropyl ether(DIPE) 0155 05 MRL ND UGIL 1 <br /> Cert-Butyl alcohol (TBA) 879 20 MRL ND UGIL 1 <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES <br /> Toluene-d8 76-129 SLSA 925% 1 <br /> 1,2-Dichloroethane-d4 53-141 SLSA 945% 1 <br /> i <br /> Approved by — Date 73) <br />