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QAIep ort <br /> Matrix Spike/Duplicate Matrix Spike Summary <br /> Castle Analytical Laboratory, Atwater, CA <br /> Lab Report No H3082101 Date 08/29/2003 Page 2 <br /> QC Batch VWMS-8283 Protect Name Lab Generated or Non COE Sample <br /> Matrix Water Protect No Late Generated or Non COE Sample <br /> Lab Samp ID VWMS-8283 Field 1D Lab Generated or Non COE Sample <br /> Basis Not Filtered Lab Ref ID 6004-6WQ <br /> Acceptance <br /> Analysis Spike Level Sample Spike Result % Recoveries Criteria <br /> Analyte Method MS DMS Result MS DMS Units MS DMS RPD % Rec RPD <br /> 1,2-01bromoethane 8260FA 250 250 ND 246 259 UGIL 984 104 55 127-76 MSA 20MSP <br /> 1,2-Dichloroethane 8260FA 25 25 U05 273 244 UG1L 107 952 12 124.70 MSA 20LSP <br /> DE-Isopropyl ether(DiPE) 6260FA 25 25 006 224 201 UGIL 872 780 11 151-51 MSA 20LSP <br /> Ethyl tert-butyl ether(ETRE) 8260FA 250 250 ND 239 158 UGIL 956 632 411 13857 MSA 201-SP <br /> Methyt-tert-butyl ether(MTBE) 8260FA 25 25 Q14 209 174 UGIL 780 640 20 12752 MSA 20 LSP <br /> tert-Amyl methyl ether(TAME) 8260FA 25 25 023 251 174 UGIL 912 604 411 122.60 MSA 20LSP <br /> tert-Butyl alcohol(TBA) 8260FA 75 0 750 2-66 4398 6628 UGIL 551 848 421 168-42 MSA 20LSP <br /> 1,2-DIchloroethane-d4 8250FA 100 100 1017 1122 1108 PERCENT 112 111 090 14153 SMSA 20SMSP <br /> Toluene-d8 8260FA 100 100 1 103.4 1020 947 PERCENT 102 947 74 129-76 SMSA 20SMSP <br />