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Castle Analytical Laboratory,Atwater, CA <br /> Lab Report No H3051601 Date 05/27/2003 Page 3 <br /> Project Name SUPER STOP MARKET Analysis Volatile Organic Compounds by GC/MS Fuel <br /> Project No 6622 Method 8260FA <br /> Prep Meth SW5030B <br /> i <br /> Field ID MW-2 Lab Samp ID 5742-2W <br /> Descr/Location MW-2 Recd Date 05/16/2003 <br /> Sample Date 05/15/2003 Prep Date 05/21/2003 <br /> Sample Time 1115 Analysis Date 05121/2003 <br /> Matrix Water QC Batch VWMS-5213 <br /> Basis Not Filtered Notes <br /> ' Analyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> Methyl-tert-butyl ether(MTBE) 0 289 05 MRL ND UGIL 1 <br /> Ethyl tert-butyl ether(ETRE) 0 084 05 MRL ND UG/L 1 <br /> tent-Amyl methyl ether(TAME) 0067 05 MRL ND UGIL 1 <br /> Di-isopropyl ether(DIPS) 0155 05 MRL ND UG/L 1 <br /> tert-Butyl alcohol (TBA) 879 20 MRL ND UGIL 1 <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES <br /> Toluene-d8 76-129 SLSA 112% 1 <br /> 1,2-Dichloroethane-d4 53.141 SLSA 108% 1 <br /> Approved by 1AL Date <br />