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Entech Analytical Labs, Inc., Santa Clara, CA <br /> Lab Report No.: H3112401 Date: 12/05/2003 Page: 3 <br /> Project Name: CARDOZA/SUPER STOP Analysis: Volatile Organic Compounds b GC/MS Fuel <br /> P y <br /> Project No: 662.2 Method: 8260FA <br /> Prep Meth: SW5030B <br /> Field ID: MW-2 Lab Samp ID: 367'03 <br /> -002 <br /> Descr/Location: MW-2 Recd Date: 11/24/2003 <br /> Sample Date: 11/21/2003 Prep Date: 11/26/2003 <br /> Sample Time: 1356 Analysis Date: 11/26/2003 <br /> Matrix: Water QC Batch: WMS310381 III <br /> Basis: Not Filtered Notes: <br /> Analyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> Methyl-tent-butyl ether(MTBE) 0.3 1- PQL ND UGIL 1 <br /> Ethyl tert-butyl ether(ETBE) 0.5 5. PQL ND UG/L 1 <br /> tert-Amyl methyl ether(TAME) 0.3 5. PQL ND UGIL 1 <br /> Di-isopropyl ether(DIPE) 0.5 5. PQL ND UG/L 1 <br /> ten-Butyl alcohol (TBA). 3. 10. PQL ND UG/L 1 <br /> 1,2-Dichloroethane 0.3 5. PQL ND UGIL 1 <br /> 1,2-Dibromoethane 0.5 5. PQL ND UGIL 1 <br /> Ethanol (EtOH) 100. 100. PQL ND UG/L 1 <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES: <br /> 4-Bromofluorobenzene 65-135 SMEA 97.4% 1 <br /> f- Toluene-d8 77-150 SMSA 105.8% 1 <br /> Dlbromofluoromethane 57-156 SMEA 102.1% 1 <br /> I <br /> } <br />� f <br /> I <br /> y Approved by: � Date: UL S 10-3 <br />