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Entech Analytical Labs, Inc., Santa Clara, CA <br /> Lab Report No.: H3112401 Date: 12/05/2003 Page: 1 <br /> Project Name: CARDOZA/SUPER STOP Analysis: Volatile Organic Compounds by GC/MS Fuel '. <br /> Project No: 662.2 Method: 8260FA <br /> Prep Meth: SW5030B <br /> Field ID: MW-1 Lab Samp ID: 36703-004 <br /> Descr/Location: MW-1 Recd Date: 11/24/2003 <br /> Sample Date: 11/2-1/2003 Prep Date: 11/28/2003 <br /> ' Sample Time: 1456 Analysis Date: 11/28/2003 f <br /> Matrix: Water QC Batch: WMS310388 J <br /> Basis: Not Filtered Notes: <br /> Analyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> Methyl-tent-butyl ether(MTBE) 3. 10. PQL 72Q UGIL 10 <br /> Ethyl tert-butyl ether(ETBE) 5. 50. PQL ND UGIL 10 <br /> tert-Amyl methyl ether(TAME) 3. 50. PQL ND UGIL 10 <br /> Di-isopropyl ether(DIPE) 5. 50. PQL ND UG/L 10 <br /> tert-Butyl alcohol (TBA) 30. 100. PQL ND UGIL 10 <br /> 1,2-Dichloroethane 3. 50. PQL ND UGIL 10 <br /> 1,2-Dlbromoethane 5. 50. PQL ND UGIL 10 <br /> Ethanol (EtOH) .1000. 1000. PQL ND UG/L 10 <br /> { SURROGATE AND INTERNAL STANDARD RECOVERIES: <br /> 4-Bromofluorobenzene 65.135 SM fl <br /> EA 97.4/0 1 I <br /> Toluene-d8 77150 SMSA 107.0% 1 <br /> Dibromofluoromethane 57-156 SMEA 102.5% 1 <br /> N <br /> i <br /> � F <br /> Approved by: Date: t2 <br />