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MINIMr, 4VERI_F'ICATION 1�►BURATORY ANALYSIS lis f <br /> PCB <br /> TPH-G TPH-D BTX & CL HC LOTH EDB ICRP/ 8270 <br /> 8010 8240 AES . <br /> 8015 8015 87b00 i 82A0 7420 0� <br /> co NTS 8260 8260 7421 II <br /> LEADED X X X X I <br /> GAS X <br /> UNI, GAS X <br /> DIESEL <br /> X X 4 <br /> X X <br /> KEROSENE E X <br /> X <br /> UNK FUEL X X X <br /> PROD. OIL X X <br /> i <br /> CHLOR. <br /> X X <br /> SOLVENTS <br /> NONCHLOR X e X <br /> •r <br /> SOLVENTS X <br /> WASH X X X X <br /> X <br /> USED OIL � X <br /> J f <br /> designated EPA methods described in EPA SW 846,Third Edition. A'20,'lTable 3-5tforund <br /> All analyses methods aregiendix Field Manual', ApF <br /> in SW 846, are specificallyvehicle fuels + Refer to the'SWR6B ohne and diesel).'Refer to 11-2-3 "Regional Board Staff Recommendations for <br /> detection limits of motor {8etecton limits. <br /> Initial Evaluation and Investigation of USTs" for the illtlov;ble Limit'ofdthe cointamin ant In question will be accepted, <br /> Detection Limits that remain below the MCL, STLC or <br /> hartever laboratory shall utilize the most conservative method. <br /> t LABORATORY ANALYSES TERMINOLOGY: 5030 8015 mod or GEMS 8360 <br /> TPH_a Total Petroleum Hydrocarbon,Gasoline, GCJFID ( } <br /> TPH-D <br /> Total Petroleum Hydrocarbon, Diesel, Gc;FID (3550), 8015 mod or C3 260 8260 <br /> BTX dt E <br /> Benzene,Toluene, Xylene dl: Ethyl Betu�ene, Gt;JPID 8020 or GGMS 8260 <br /> CL HC Chlorinated Hydrocarbon, GMSD 18010, GGMS 8240 <br /> TOTAL LEAD Total lead, AA 7420, AA 7421 or ICP-AES 6010 <br /> EDB Ethylene dlbromide {DHS-AB 1803); GCJMS 8240 (DHS-LUFn <br /> CC-FID <br /> Cttramatogtaphy, Flame Ionixaflon Detection <br /> ]CAP or AA Inductively Coupled Plasma Atomic'IEmisslon Spectrometry 6010 or Atomic Absorption <br /> Spectrometry 7000. Metals% Cadmium, Chromium H1 and VI, Lead, Zinc.and Nickel. <br /> PCB Polychlorinated Biphenyls, GMS 8270 or 8080 <br /> Method 3050 Acid digestion <br /> Method 3540 Sozhlet sample preparation <br /> Method 3550 Sonicatlon sample preparation, extraction method <br /> Method 5030 Purge and trap sample preparation ; <br /> QA/QC Quality AssuranWQualiry Control <br /> avoid false hive detection of benzene,benzene-tree solvents are to be used. Fused capillary columns are <br /> Notes. To P� <br /> P <br /> referred to packed columns; a packed column may be used <br /> a"[last cut"with 'dirty" samples yr coos We hydrocarbons <br /> have been characterized and proper QA/AC is followed. <br /> For Drinking water sources, EPA recommends that the 500� erles for volatile organics be used in.preferenoe to the 600 <br /> ting any level of heavy m <br /> series because the detection limits ate lower and the QA/QC mends holdingpthese sles amiples until disposal is indicated. <br /> contamination may require further analysis. PHS-EHD recom <br /> Page 8 <br /> EH 23 048 (Revised 7110/'92) <br /> F <br />