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Alpha Analytical, Inc. <br /> 255 Glendale Ave. - Suite 21 • Sparks,Nevada 89431-5778 <br /> (775) 355-1044 • (775) 355-0406 FAX • 1-800-283-1183 <br /> Date: <br /> Work Order: <br /> 25-Nov-02 QC Summary Report 02111220 <br /> Method Blank Type MBLK Test Code: SW826013 Batch ID: MS09W1113A <br /> Fife ID: D:IHPCHEM1MS091DATA1021113102111307.D Analysis Date: 111131200210:16 <br /> Sample ID: MBLK MS09W1113A Units: NgIL Run ID:GCIMSD_9_021113A Prep Date: 11/1312002 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit Hightimit RPD Ref Val %RPD Qual <br /> Tertiary Butyl Alcohol (TBA) ND 5 <br /> Methyl tert-butyl ether(MTBE) ND 0.5 <br /> Di-isopropyl Ether(DIPE) ND 1 <br /> Ethyl Tertiary Butyl Ether(ETRE) ND 1 <br /> Benzene ND 0.5 <br /> Tertiary Amyl Methyl Ether(TAME) ND 1 <br /> Toluene ND 0.5 <br /> Ethylbenzene ND 0.5 <br /> m,p-Xylene ND 0.5 <br /> o-Xylene ND 0.5 <br /> Surr. 1,2-Dichloroethane-d4 10 10 100 71 130 <br /> Surr.Toluene-d8 9.85 10 99 69 127 <br /> Surr:4-Bromofluorobenzene 9.46 10 95 80 123 <br /> Laboratory Control Spike Type LCS Test Code: SW8260B Batch ID: MS09WI113A <br /> File ID: D:IHPCHEM\MS09\DATAX021113102111304.D Analysis Date: 111131200209:07 <br /> Sample ID: LCS MS09W1113A Units : NgIL Run ID: GC/MSD-9_021113A Prep Date: 1111312002 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit Hightimit RPD Ref Val %RPD Qual <br /> Benzene 10.6 0.5 10 106 80 120 <br /> Toluene 10.3 0.5 10 103 80 120 <br /> Ethylbenzene 10.4 0.5 10 104 80 120 <br /> m,p-Xylene 20.3 0.5 20 102 73 129 <br /> OXylene 10.6 0.5 10 106 73 127 <br /> urr: 1,2-Dichloroethane-d4 9.81 10 98 71 130 <br /> Surr:Toluene-d8 9.98 10 99.8 69 127 <br /> Surr:4-Bromofluorobenzene 10.3 10 103 80 123 <br /> Sample Matrix Spike Type MS Test Code: SW8260B Batch ID: MS09W1113A <br /> File ID: D:kHPCHEM1MS091DATA1021113102111314.D Analysis Date: 11/13/2002 12:57 <br /> Sample ID: 02111242-04AMS Units: pg1L Run ID: GCIMSD_9_021113A Prep Date: 11113/2002 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit Hightimit RPD Ref Val %RPD Qual <br /> Benzene 54.3 1.3 50 0 109 80 120 <br /> Toluene 52.3 1.3 50 0 105 80 120 <br /> Ethylbenzene 52.7 1.3 50 0 105 80 120 <br /> m,p-Xylene 104 1.3 100 0 104 73 129 <br /> o-Xylene 53.6 1.3 50 0 107 73 127 <br /> Surr:1,2-Dichloroethane-d4 49.2 50 98 71 130 <br /> Surr:Toluene-d8 49.8 50 99.5 69 127 <br /> Surr:4-Bromofluorobenzene 49.5 50 99 80 123 <br /> Sample Matrix Spike Duplicate Type MSD Test Code: SW8260B Batch ID: MS09W1113A <br /> File ID: D;IHPCHEM1MS091DATA1021113102111315.D Analysis Date: 11113/200213:20 <br /> Sample ID: 02111242-04AMSD Units: pg1L Run ID: GCIMSD_9_021113A Prep Date: 11/13/2002 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit Hightimit RPD Ref Val %RPD Qual <br /> Benzene 53.6 1.3 50 0 107 80 120 54.25 1.15 <br /> Toluene 51.7 1.3 50 0 103 BO 120 52.34 1.21 <br /> Ethylbenzene 52.2 ....... 1.3 = 50 _ - 0 ..104 80 ,_ _ 120 52.65 0.954. . . <br /> m,p-Xylene 103 1.3 100 0 103 73 129 103.5 0.329 <br /> o-Xylene 53.5 1.3 50 0 107 73 127 53.56 0.0373 <br /> Surr. 1,2-Dichloroethane-d4 49.2 50 98 71 130 <br /> Surr;Toluene-d8 49.5 50 99 69 127 <br /> Surr;4-Bromofluorobenzene 50.9 50 102 80 123 <br /> AIML <br /> omments: ND-Not Detected at the Reporting Limit. D-If the spiked value is<25%of the reference value,recovery should not be calculated. <br /> S-Spike Recovery outside accepted recovery limits. M-Spike Recovery outside accepted recovery limits due to matrix. <br /> B-Analyte detected in the associated Method Blank. <br />