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Alpha Analytical, Inc. <br /> 255 Glendale Ave. • Suite 21 • Sparks,Nevada 89431-5778 <br /> (775)355-1044•(775)355-0406 FAX• 1-800-283-1183 <br /> Date: <br /> 22-Apr-04 QC Summary Report Work Order: <br /> 0444]240 <br /> Method Blank Type MBLK Test Code: EPA Method SW826oa <br /> File ID: D:\HPCHEM1MS081DATA1040413104041305.D Batch ID: MS08WO413A Analysis Date: 04/13/2004 12:56 <br /> Sample ID: MBLK MS08WO413A Units: pg/L Run ID:GC/MSD 8_040413A Prep Date: 04/13/2004 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPDRefVal %RPD(Limit) Qua[ <br /> Tertiary Butyl Alcohol[TBA) ND 5 <br /> Methyl tert-butyl ether(MTBE) ND 0.5 <br /> D[-isopropyl Ether(DIPE) ND 1 <br /> Ethyl Tertiary Butyl Ether(ETBE) ND 1 <br /> Benzene ND 0.5 <br /> Tertiary Amyl Methyl Ether(TAME) ND t <br /> Toluene ND 0.5 <br /> Ethylbenzene ND 0.5 <br /> m,p-Xylene ND 0.5 <br /> o-Xylene ND 0.5 <br /> Surr:1,2-Dichloroethane-d4 11.1 10 ill 72 126 <br /> Surr:Toluene-d8 10.4 10 104 71 128 <br /> Surr:4-Bromofluorobenzene 10.5 10 105 76 121 <br /> Laboratory Control Spike Type LCS Test Code: EPA Method SW8260B <br /> File ID: D:IHPCHEM1MS081DATA1040413104041303.D Batch ID: MS08WO413A Analysis Date: 04/13/2004 12:14 <br /> Sample ID; LCS MS08W0413A Units: pg/L Run ID:GC/MSD_8_040413A Prep Date: 04/13/2004 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowUmit Higl LUm€t RPDRefVal %RPD(Limit) Qua] <br /> Benzene 8.53 0.5 10 85 83 119 <br /> Toluene 9.63 0.5 10 96 80 120 <br /> Ethylbenzene 9.39 0.5 10 94 80 120 <br /> m,p-Xylene 9.47 0.5 10 95 77 125 <br /> xylene 9.59 0.5 10 96 77 124 <br /> "...rr: 1,2-Dichloroethane-d4 11.7 10 117 72 126 <br /> Surr:Toluene-d8 10.4 10 104 71 128 <br /> Surr:4-Bromofluorobenzene 9.54 10 95 76 121 <br /> Sample Matrix Spike Type MS Test Code: EPA Method SW8260B <br /> File ID: D:IHPCHEMIMS08IDATAI0404i3104041306.D Batch€D: MS08WO413A Analysis Date: D4/13/2004 13:18 <br /> Sample ID: 04041240-01AMS Units: pg/L Run ID:GC/MSD-8-040413A Prep Date: 04/13/2004 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowUmit HighLimit RPDRefVal %RPD(Limit) Qual <br /> Benzene 43.6 1.3 50 0 87 59 145 <br /> Toluene 48.8 1.3 50 0 98 39 161 <br /> Ethylbenzene 47.9 1.3 50 0 96 57 145 <br /> m,p-Xylene 48.3 1.3 50 0 97 37 163 <br /> o-Xylene 48.8 1.3 50 0 98 47 156 <br /> Surc 1,2-Dichloroethane-d4 57,2 50 114 72 126 <br /> Surr:Toluene-d8 51 50 102 71 128 <br /> Surr:4-Bromof€uorobenzene 47.6 50 95 76 121 <br /> Sample Matrix Spike Duplicate Type MSD Test Code: EPA Method SW8260B <br /> File ID: D:\HPCHEMIMSOSIDATA1040413104041307.D Batch ID: MS08W0413A Analysis Date: 04/13/2004 13:39 <br /> Sample ID: 04041240-01AMSD Units: pg/L Run ID:GC/MSD_8_040413A Prep Date: 04/13/2004 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPDRefVal %RPD(Limit) Qual <br /> Benzene 46 1.3 50 0 92 59 145 43.64 5.2(22) <br /> Toluene 51 1.3 50 0 102 39 161 48.81 4,4(22) <br /> Ethylbenzene 50.1 1.3 50 0 100 57 145 47,93 4.4(22) <br /> m,p-Xylene 50.8 1.3 50 0 102 37 163 48.25 5.2(23) <br /> o-Xylene 51.5 1,3 50 0 103 47 156 48.77 5.5(50) <br /> Surr: 1,2-Dichloroethane-d4 56.1 50 112 72 126 <br /> Surr:Toluene-d8 50.7 50 101 71 128 <br /> Surr:4-Bromofluorobenzene 47,2 50 94 76 121 <br /> tor <br /> � rents: <br /> "culations are based off of raw(non-rounded)data.However,for reporting purposes,all QC data is rounded to three significant figures.Therefore,hand calculated <br /> values may differ slightly. <br />