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Alpha Analytical, Inc. <br /> ( 255 Glendale Ave. • Suite 21 -Sparks,Nevada 89431-5778 <br /> (� (775)355-1044• (775)355-0406 FAX • 1-800-283-1183 <br /> 01) <br /> ate: Work Order: <br /> a-oct-05 OC Summary Report 05100702 <br /> Method Blank Type:11ABLK Test Code: EPA Method SW8260B <br /> File ID: D:IMSDCHEM1MS121DATA1051007105100706.D Batch ID;MS12A1007A Analysis Date: 10107/2005 12:08 <br /> Sample ID: MBLK MS12A1007A Units : mglm' Run ID:MSD_12_05100713 Prep Date: 10107/2005 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPDRefVal %RPD(Limit) Qual <br /> Tertiary Butyl Alcohol(TBA) ND 5 <br /> Methyl tert-butyl ether(MTBE) NO 0.1 <br /> Di-isopropyl Ether(DIPE) NO 0.2 <br /> Ethyl Tertiary Butyl Ether(ETBE) NO 0.2 <br /> Benzene NO 0.1 <br /> Tertiary Amyl Methyl Ether(TAME) ND 0.2 <br /> Toluene NO 0.1 <br /> Ethylbenzene ND 0.1 <br /> m,p-Xylene ND 0.1 <br /> o-Xylene NO 0.1 <br /> Surr. 1,2-Dichloroethane-d4 2.08 2 104 76 127 <br /> Surr:Toluene-d8 1.91 2 96 84 113 <br /> Surr:4-Bromofluorobenzene 1.97 2 99 79 119 <br /> Laboratory Control Spike Type:LCS Test Code: EPA Method SW8260B <br /> File ID: D:IMSDCHEM\MS121DATA1051007105100703.D Batch ID:MS12A1007A Analysis Date: 1010712005 11:03 <br /> Sample 10: LCS MS12A1007A Units :mglm' Run ID:MSD_12_051007B Prep Date: 1010712005 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl.imit HighLimit RPDRefVai %RPD(Limit) Qual <br /> Benzene 10.9 0.1 10 109 81 122 <br /> Toluene 9.87 0.1 10 99 80 120 <br /> Ethylbenzene 10.5 0.1 10 105 80 120 <br /> m,p-Xylene 10.6 0.1 10 106 80 129 <br /> o-Xylene 10.9 0.1 10 109 80 129 <br /> orr: 1,2-Dichloroethane-d4 10.9 10 109 76 127 <br /> urc Toluene-d8 9.48 10 95 84 113 <br /> Surr:4-Bromofluoro benzene 9.91 10 99 79 119 <br /> Comments: <br /> Calculations are based off of raw(non-rounded)data.However,for reporting purposes,all QC data is rounded to three significant figures.Therefore,hand calculated <br /> values may differ slightly. <br />