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Alpha Analytical, Inc. <br /> ( +�YA 255 Glendale Ave. • Suite 21 • Sparks, Nevada 59431-5778 <br /> (775)355-1044 • (775)355-0406 FAX • 1-800-283-1183 <br /> Work Order: <br /> Q'tc-05e: QC SuI7ll ary Report 05120804 <br /> Method Blank Type:MBLK Test Code: EPA Method SW8260B <br /> File ID: D:IMSDCHEMIMS121DATAL051209L05120935.D Batch ID:MS12A1209A Analysis Date: 12/0912005 21:51 <br /> Sample ID: MBLK MS12AI209A Units: mg/ml Run ID:MSD_12_051209B Prep Date: 92/09/2005 <br /> Anaiyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPDRefVal %RPD(Limit) Qual <br /> Tertiary Butyl Alcohol(TSA) ND 5 <br /> Methyl tert-butyl ether(MTBE) ND 0.1 <br /> Di-isopropyl Ether(RIPE) ND 0.2 <br /> Ethyl Tertiary Butyl Ether(ETBE) ND 0.2 <br /> Benzene ND 0.1 <br /> Tertiary Amyl Methyl Ether(TAME) ND 0.2 <br /> Toluene ND 0.1 <br /> Ethyibenzene ND 0.1 <br /> m,p-Xylene ND 0.1 <br /> o-Xylene ND 0.1 <br /> Surr: 1,2-Dichloroethane-d4 2.05 2 103 76 127 <br /> Surr.Toluene-d8 1.94 2 97 84 113 <br /> Surr:4-Bromofluorobenzene 1.85 2 93 79 119 <br /> Laboratory Control Spike Type:LCS Test Code: EPA Method SW8260B <br /> File ID:D.IMSDCHEMIMS121DATA1051209105120932.D Batch ID:MS12A1209A Analysis Date: 12/09/2005 20:47 <br /> Sample ID: LCS MS12A1209A Units :mg/ml Run ID:MSD_12_051209B Prep Date: 12/09/2005 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPDRefVal %RPD(Limit) Qual <br /> Benzene 9.57 0.1 10 96 81 122 <br /> Toluene 8.89 0.1 10 89 80 120 <br /> Ethylbenzene 9.55 0.1 10 96 80 120 <br /> m,p-Xylene 9.62 0.1 10 96 80 129 <br /> ene 9.95 0.1 10 100 80 129 <br /> 1,2-Dichloroethane-d4 10.7 10 107 76 127 <br /> Toluene-d8 9.63 10 96 84 113 <br /> Surr:4-B romofl uoro benzene 9.67 10 97 79 119 <br /> Comments: <br /> Calculations are based off of raw(non-rounded)data.However,for reporting purposes,all QC data is rounded to three significant figures.Therefore,hand calculated <br /> values may differ slightly. <br /> i <br />