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Alpha Analytical, Inc. <br /> I 255 Glendale Ave.• Suite 21 •Sparks,Nevada 89431-5778 <br /> I� (775)355-1044• (775)355-0406 FAX• 1-800-283-1183 <br /> Ottate: Work Order: <br /> 05 OC Summary Report 05051201 <br /> Method Blank Type MBLK Test Code: EPA Method SW8260B <br /> File ID: D:IMSDCHEM1MS121DATA1050512105051241.D Batch ID:MS12AO512A Analysis Date: 05/12/2005 22:41 <br /> Sample ID: MBLK MS12AO512AB Units: mg/M3 Run ID:MSD_12_050512A Prep Date: 05/12/2005 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPDRefVal %RPD(Limit) Qual <br /> Tertiary Butyl Alcohol(TBA) ND 5 <br /> Methyl tert-butyl ether(MTBE) ND 0.1 <br /> Di-isopropyl Ether(DIPS) ND 0.2 <br /> Ethyl Tertiary Butyl Ether(ETBE) ND 0.2 <br /> Benzene ND 0.1 <br /> Tertiary Amyl Methyl Ether(TAME) ND 0.2 <br /> Toluene ND 0.1 <br /> Ethylbenzene ND 0.1 <br /> m,p-Xylene ND 0.1 <br /> o-Xylene ND 0.1 <br /> Surr: 1,2-Dichloroethane-d4 1.96 2 98 76 127 <br /> Surr:Toluene-d8 1.91 2 96 84 113 <br /> Surr:4-Bromofluorobenzene 2 2 100 79 119 <br /> Laboratory Control Spike Type LCS Test Code: EPA Method SW8260B <br /> File ID: D:WSDCHEMWS121DATA1050512105051238.D Batch ID.MS12AO512A Analysis Date: 05/12/2005 21:38 <br /> Sample ID: LCS MS12A0512A M Units: mglm3 Run ID:MSD_12_050512A Prep Date: 05/12/2005 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPDRefVal %RPD(Limit) Qual <br /> Benzene 9.05 0.1 10 91 81 122 <br /> Toluene 8.7 0.1 10 87 80 120 <br /> Ethylbenzene 9.22 0.1 10 92 80 120 <br /> m,p-Xylene 9.34 0.1 10 93 80 129 <br /> o-Xylene 9 0.1 10 90 80 129 <br /> rr:1,2-Dichloroethane-d4 10.2 10 102 76 127 <br /> rr:Toluene-d8 9.79 10 98 84 113 <br /> urr:4-Bromofluorobenzene 10.3 10 103 79 119 <br /> Comments: <br /> Calculations are based off of raw(non-rounded)data.However,for reporting purposes,all QC data is rounded to three significant figures.Therefore,hand calculated <br /> values may differ slightly. <br />