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Date: <br /> zg-Mayoo P Y Alpha Analytical, Inc. - QC Summary Report Work Order: <br /> 00051944 <br /> Method Blank Test Code: SW8015 Batch ID: MS8W0517B Anaiysis date: 05118/2000 15:48 <br /> Sample 1D: MBLK 00051806 Units: mglL Run la: GCIMSD 8 000517 Prep Date: 05N812000 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit Hight.imit RPD Ref Val %RPD Qual <br /> TPH Purgeable ND 0.05 <br /> IL�r: 1,2-Dichloroethane-d4 0.0108 0.01 108 68 139 <br /> rr:Toluene-d8 0.00942 0.01 94 75 127 <br /> Sum 4-Bromofluorobenzene 0.0103 0.01 103 73 128 <br /> I <br /> Laboratory Control Spike Test Code: SW8015 Hatch ID: MS8W051713 Analysis Date: 0511 912000 12:29 <br />' Sample ID: GLCS MS8W0517B Units: mg1L Run ID: GCIMSD 8_000517 Prep Date: 05/19/2000 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit Hight-imit RPD Ref Val %RPD Qual <br /> TPH Purgeable 0.351 0.05 0.4 88 63 140 { <br /> Surr: 1,2-Dichloroethane-d4 0.0107 0.01 107 68 139 <br /> Surr:Toluene-d8 0.00955 0.01 96 75 127 <br /> Surr:4-Bromofluorobenzene 0.0102 0.01 102 73 128 <br /> Sample Matrix Spike Test Code: SW8015 Batch 1D: MS8W0517B Analysis Date: 05/19/2000 07:12 <br /> Sample ID: 00051646-0BAGS Units: mglL Run ID: GC/MSD_8_000517 Prep Date: 05119/2001) <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPD Ref Val %RPD Qual <br /> TPH Purgeable 2.03 0.25 2 0.277 88 63 140 <br /> Surr:1,2-Dichloroethane-d4 0.0504 0.05 101 68 139 <br /> Surr.Toluene 8 r0.0478 0.05 96 75 127 <br /> Surr:4-Bromofluorobenzene 0.0528 0.05 106 73 128 <br /> i <br /> Sample Matrix Spike Duplicate Test Code: SW8015 Batch ID: MS8W051713 Analysis Date: 05/19/2000 07:38 <br /> Sample ID: 00051646-08AGSD Units: mglL Run ID: GCIMSD_8_000517 Prep Date: 0511912000 <br /> Analyte Result PQL SpkVal SpkReNal %REC LowLimit HighLimit RPD Ref Val %RPD Qua! <br /> TPH Purgeable 1.95 0.25 2 0.277 '84 63 140 2.028 4.07 <br /> Surr: 1,2-Dichioroethane�d4 0.0519 0.05 104 68 139 <br /> Surr:Toluene-d8 0.0478 0.05 96 75 127 <br /> Surr:4-Bromofluorobenzene 0.0517 0.05 103 73 128 <br /> I <br /> i <br /> ^,mments: ND-Not Detected at the Reporting Limit. D-If the spiked value is<25%of the reference value recoveryshould not be calculated. <br /> u ted. <br /> S-Spike Recovery outside accepted recovery limits. M-Spike Recovery outside accepted recovery limits due to matrix. <br /> B-Analyte detected in the associated Method Blank. <br /> L <br />