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Alpha Analytical, Inc. <br /> 255 Glendale Ave. • Suite 21 •Sparks,Nevada 89431-5778 <br /> (775)355-1044 •(775)355-0406 FAX• 1-800-283-1183 <br /> Date: Work Order: <br /> 19-Jan-04 QC Summary Report 04010947 <br /> Method Blank Type MBLK Test Code: EPA Method SW8260B <br /> File ID: D:IMSDCHEM1MS121DATA1040114104011406.D Batch ID: MS12W0114A Analysis Date: 01/14/2004 09:56 <br /> Sample 1D: MBLK MS12W0114A Units: Ng/L Run ID:GC/MSD_12 040114A Prep Date: 01/14/2004 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLim[t RPDRefVal %RPD(Umit) Qual <br /> Tertiary Butyl Alcohol (TBA) ND 5 <br /> Methyl tert-butyl ether(MTBE) ND 0.5 <br /> Di-isopropyl Ether(DIPE) ND 1 <br /> Ethyl Tertiary Buts]Ether(ETRE) ND 1 <br /> Benzene ND 0.5 <br /> Tertiary Amyl Methyl Ether(TAME) ND 1 <br /> Toluene ND 0.5 <br /> Ethylbenzene ND 0.5 <br /> m,p-Xylene ND 0.5 <br /> o-Xylene ND 0.5 <br /> Surr: 1,2-Dichloroethane-d4 10.7 10 107 72 126 <br /> Surr:Toluene-d8 9.99 10 99.9 71 128 <br /> Surr 4-Bromofluorobenzene 9.14 10 91 76 121 <br /> Laboratory Control Spike Type LCS Test Code: EPA Method SW8260B <br /> File ID: D:\MSDCHEM\MS12\DATA\040114\04011404.D Batch ID: MS12W0114A Analysis Date: 01/14/2004 09:14 <br /> Sample ID: LCS MS12W0114A Units: NgIL Run ID:GC/MSD-12-040114A Prep Date: 01/14/2004 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPDRefVal %RPD(Umit) Qual <br /> Benzene 9.85 0.5 10 99 83 119 <br /> Toluene 9.64 0.5 10 96 80 120 <br /> Ethylbenzene 9.73 0.5 10 97 80 120 <br /> p-Xylene 21.6 0.5 20 108 77 125 <br /> \,,,Cylene 10 0.5 10 100 77 124 <br /> Surr:1,2-Dichloroethane-d4 10.8 10 108 72 126 <br /> Surr:Toluene-d8 9.9 10 99 71 128 <br /> Surr:4-Bromofluorobenzene 8.75 10 88 76 121 <br /> Sample Matrix Spike Type MS Test Code: EPA Method SW8260B <br /> File ID: D:\MSDCHEM1MS121DATA1040114104011407.D Batch ID: MS12WO114A Analysis Date: 01/14/2004 10:17 <br /> Sample ID: 04010947-01AMS Units: NgIL Run ID:GCIMSD_12 040114A Prep Date: 01/14/2004 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowUmit HighLimit RPDRefVal %RPD(Limit) Qua] <br /> Benzene 51.2 1.3 50 0 102 59 145 <br /> Toluene 49 1.3 50 0 98 39 161 <br /> Ethylbenzene 49 1.3 50 0 98 57 145 <br /> m,p-Xylene 110 1.3 100 0 110 37 163 <br /> o-Xylene 51.2 1.3 50 0 102 47 156 <br /> Surr:1,2-Dichloroethane-d4 53.7 50 107 72 126 <br /> SUM Toluene-dB 50 50 100 71 128 <br /> Surr:4-Bromofluorobenzene 43.9 50 88 76 121 <br /> Sample Matrix Spike Duplicate Type MSD Test Code: EPA Method SW8260B <br /> File ID: D:IMSDCHEMIMS121DATA104011410401140B.D Batch]D: MS12W0114A Analysis Date: 01/14/2004 10:38 <br /> Sample ID: 04010947-01AMSD Units: NgIL Run[D:QC/MSD_12_040114A Prep Date: 01/14/2004 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighUrnit RPDRefVal %RPD(Limit) Qua[ <br /> Benzene 50.4 1.3 50 0 101 59 145 51.24 1.6(22) <br /> Toluene 48.6 1.3 50 0 97 39 161 48.95 0.7(22) <br /> Ethylbenzene 49.1 1.3 50 0 98 57 145 49.04 0.2(22) <br /> m,p-Xylene 109 1.3 100 0 109 37 163 110.4 0.8(23) <br /> o-Xylene 51.2 1.3 50 0 102 47 156 51.15 0.1(50) <br /> Surr: 1,2-Dichloroethane-d4 52.1 50 104 72 126 <br /> Surr;Toluene-d8 49.8 50 99.7 71 126 <br /> Surr:4-Bromofluorobenzene 43.5 50 87 76 121 <br /> %,yomments. <br /> Calculations are based off of raw(non-rounded)data.However,for reporting purposes,all QC data is rounded to three significant figures.Therefore,hand calculated <br /> values may differ slightly. <br />