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07/21/2004 14:23 209572091.6 GEO PAGE 05/15 <br /> i <br /> GeoAnalytical LaboratoriesInc. <br /> 1405 Kansas Avenue Modesto,CA 95351 Phone(209)572-0900 Fax (209)572-0916 ' <br /> Report# Q184-08 CERTIFICATE OF ANALYSIS Date: 7/12/04 <br /> Thorpe Oil Date Rec'd: 7/02/04 <br /> PO Box 357 Project- 601 E.Main St.-Stockton Date Started: 7/08/04 <br /> Lodi CA 95241 Date Completed:7/08/04 <br /> pO# Date Sampled: 7/02/04 <br /> Sample ID: SP-1,2 Time: <br /> Lab ID: Q200946,Q200947 Sampler : R.Bombaywala(Geo) <br /> Method RL Anal to Results Units <br /> 8260H 50 Benzene <br /> 5.0 Toluene ND kg/Kg <br /> ND <br /> 5.0 Ethyl Benzene ND <br /> 5.0 Total Xylenes ND <br /> 10 Methyl tert-butyl ether(MTBE) ND <br /> 400 Ethanal ND <br /> 200 tent-Butanol ND <br /> 10 di-leoprapyl ether(RIPE) ND <br /> 10 Ethyl tert-butyl ether(ETRE) ND <br /> 10 tert-Amyl methyl ether(TAME) ND <br /> Surrogate <br /> thane-d Amnt Spiked Amnt Rec. %Recovery OC Limit g4 <br /> < 20 18.9 94.5 66-133 <br /> 2-Bmmo-l-chloropropane 20 20.4 102.0 63-139 <br /> 4-Bromofluorobenzene 20 19.8 99.0 64-136 <br /> Matt Page <br /> Chemist Donna Keller <br /> Certification# 1157 Laboratory Director <br />