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07/21/2004 14:23 209572091E GED PAGE 07/15 <br /> Ge•Analytical Laboratories, Inc. <br /> 1405 Kansas Avenue Modesto,CA 95351 Phone(209)572-0900 Fax(209)572-0916 <br /> Report# Q184-08 CERTIFICATE OF ANALYSIS Date: 7/12/04 <br /> Thorpe Oil Date Recd: 7/02/04 <br /> PO Box 357 Project: 601 E, Main St.-Stockton Date Started: 7/08/04 <br /> Lodi CA 95241 Date Completed:7/08/04 <br /> PO# Date Sampled: 7/02/04 <br /> Sample ID: TK-2 Time: <br /> Lab ID: Q200949 Sampler; R.Bombaywala(Geo) <br /> Method RL Anai to Results Units <br /> 82608 5.0 Benzene ND µg/Kg <br /> 5.0 Toluene <br /> ND <br /> 5.0 Ethyl Benzene 8.6 <br /> 5.0 Total Xylenes 31 <br /> 10 Methyl tert-butyl ether(MTBE) ND <br /> 400 Ethanol ND <br /> 200 tert-Butanol ND <br /> 10 di-Isopropyl ether(DIPE) ND <br /> 10 Ethyl Cert-butyl ether(ETBE) ND <br /> 10 tert-Amyl methyl ether(TAME) NO <br /> Surrogate Amnt Spiked Amnt Rea %Recovery OC Limit <br /> 1,2-Dichioroethane-d, 20 31.4 157.0 66-133 <br /> 2-Bromo-l-chloropropane 20 26.1 130.5 63-139 <br /> 4-Brotnoflaorobenzene 20 27.6 138.0 64-136 <br /> Matt Page <br /> ChemistDonna Keller <br /> Certification # 1157 Laboratory Director <br />