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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> 64h //www mccam bell coin E-mail main@mccampbell corn <br />' Advanced GeoEnvironmental Client Project ID National Freight Date Sampled 05/31/01 <br /> 837 Shaw Road Date Received 06/01/01 <br />' Stockton, CA 95215 Client Contact Paul Dotson Date Extracted 06/01-06/06/01 <br /> Client P O Date Analyzed 06/01-06/06/01 <br />' Seven Oxygenated Volatile Organics By GCIMS <br /> EPA method 8260 modified <br /> Lab ID 68792 68793 68794 <br /> MW1/ MW2/ MW3/ Reporting Limit <br /> Client ID 05-31-01 05-31-01 05-31-01 <br />' Matrix W W W S W <br /> Compound Concentration* ug/kg ug/L <br />' Di-isopropyl Ether(DIPS) ND ND ND 50 10 <br /> Ethyl tert-Butyl Ether(ETRE) ND ND ND 50 10 <br /> Methyl tert-Butyl Ether(MTBE) ND ND ND so 10 <br /> tert-Amyl Methyl Ether(TAME) ND ND ND 50 10 <br /> ' tert-Butanol ND ND ND 25 50 <br /> ' Methanol ND ND ND 1000 500 <br /> Ethanol ND ND ND 250 50 <br /> Surrogate Recoveries(%) <br /> ' Dibromofluoromethane 103 109 log <br /> ' Comments h <br /> *water samples are reported in ug/1.,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,NIA means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present,(i)liquid sample that contains greater than—5 vol %sediment,0)sample diluted due to <br /> high organic content <br /> DHS Certification No 1644 Edward Hatrulton,Lab Director <br /> 1 <br />