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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> ht //www mccam bell e m E-mail main@mccatnpbell com <br /> Advanced GeoEnvuonmental Chent Protect ID National Freight Date Sampled 03/15/01 <br /> ' 837 Shaw Road Date Received 03/16/01 <br /> Stockton,CA 95215 Client Contact Paul Dotson Date Extracted 03/16-03/22/01 <br /> ' Client P O Date Analyzed 03/16-03/22/01 <br /> EPA method 8260 modified 7 Oxygenated Volatile Organics By GC/MS <br /> Lab ID 62941 62942 62943 <br /> Reporting Lima <br /> Client ID MWl/03-15-01 MW2/03-15-01 MW3/03-15-01 <br /> ' Matrix W It W W S W <br /> Compound Concentration* ug/kg ug/L <br /> ' <br /> —Di-isopropyl Ether(RIPE) ND ND ND so 10 <br /> ' Ethyl tert-Butyl Ether(ETBE) ND ND ND so 10 <br /> Methyl-tert Butyl Ether(MTBE) ND ND ND 50 10 <br /> tert-Amyl Methyl Ether(TAME) ND ND ND 50 10 <br /> tert-Butanol ND ND ND 25 50 <br /> ' Methanol ND ND ND 1000 200 <br /> ' Ethanol ND ND ND 250 50 <br /> Surrogate Recoveries(%) <br /> ' Dibromofluoromethane 98 107 105 <br /> ' Comments h <br /> *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,N/A means surrogate not applicable to this analysts <br /> (h)lighter than water imn-ascible sheen is present,(i)liquid sample that contains greater than–5 vol %sediment,0)sample diluted due to <br /> high organic content <br /> DHS Certification No 1644 <br /> Edward Hamilton,Lab Director <br />