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110 2nd Avenue South,#137,Pacheco,CA 94553-5560 <br /> ' 14 hap MCCANOBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> /lwww.mccamnbell com E-mail main@mccampbell com <br /> Advanced GeoEnvironmental Client Project ID National Freight Date Sampled 09/02/99 <br /> 4005 North Wilson Way Date Received 09/04/99 <br /> Stockton,CA 95205 Client Contact Tun Cuellar Date Extracted 09/04/99 <br /> ' Client P O Date Analyzed 09108-09/10/99 <br /> Diesel Range(C10-C23)Extractable Hydrocarbons as Diesel * <br /> EPA methods modified 8015,and 3550 or 3510,California RWQCB(SF Bay Region)method GCFID(3550)or GCFl (3510) <br /> ' Lab ID Client ID Matrix TPH(d)r %Recovery <br /> Surrogate <br /> 18688 P1-20 S 10,000,a 98 <br /> 18692 PI-40 S 4800,a 110 <br /> 18693 P145 S 2700,a 110 <br /> 18695 P1-55 S 3100,a 110 <br /> 18696 P1-65 S 300,a 113 <br /> 18700 P2-20 S ND 109 <br /> lie 18702 P2-30 S ND 110 <br /> Reporting Limit unless otherwise W 50 ug/L <br /> stated,ND means not detected above <br /> the reporting limit S 1 0 mg/kg <br /> 'water and vapor samples are reported to ug/L.,wipe samples in ug/wipe,soil and sludge samples in mg/kg,and all TCLP I STLC I SPLP <br />' extracts in ug/l- <br /> "cluttered chromatogram resulting in coeluted surrogate and sample peaks,or,surrogate peak is on elevated baseline,or,surrogate has been <br /> diminished by dilution of ongmal extract <br /> }The following descriptions of the TPH chromatogram are cursory in nature and McCampbell Analytical is not responsible for their <br /> interpretation a)unmodified or weakly modified diesel is significant,b)diesel range compounds are significant,no recognizable pattern,c) <br /> aged diesel9 is significant),d)gasoline range compounds are significant,e)medium boding point pattern that does not match diesel (7), 0 <br /> one to a few isolated peaks present, g) oil range compounds are significant, h) lighter than water immiscible sheen is present, i) liquid <br /> sample that contains greater than--5 vol %sediment <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />