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- 819 Striker Avenue,Suite 8 <br /> TestAmerica Sacramento, 92 99600 <br /> (916)921-9600 <br /> FAX(916)921-0100 <br /> ANAtYTICAI TESTING CORPORATION <br /> www.testamericain c.com <br /> Blaine Tech Services(Shell) Project:/341 East Main Street,Ripon SQC0333 <br /> 1680 Rogers Avenue Project Number: 98995874 Reported: <br /> San Jose CA,95112 Project Manager: Jason Brown 04/09/07 12:28 <br /> Volatile Organic Compounds by EPA Method 8260B- Quality Control <br /> TestAmerica-Morgan Hill, CA <br /> Reporting Spike Source %REC RPD <br /> Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch 7C30048-EPA 5030B P/T/EPA 8260B <br /> Blank(7C30048-BLKI) Prepared:03/30/07 Analyzed:03/31/07 <br /> Benzene ND 0.50 ug/l <br /> Toluene ND 0.50 " <br /> Ethylbenzene ND 0.50 " <br /> Xylenes(total) ND 0.50 " <br /> Methyl tert-butyl ether ND 0.50 " <br /> Di-isopropyl ether ND 0.50 <br /> Ethyl tert-butyl ether ND 0.50 " <br /> tert-Amyl methyl ether ND 0.50 <br /> ten-Butyl alcohol ND 20 <br /> 1,2-Dichloroethane ND 0.50 <br /> 1,2-Dibromoethane(EDB) ND 0.50 <br /> Ethanol ND 100 <br /> Surrogate:DibromoJluoromethane 2.48 2.50 99 75-120 <br /> Surrogate:1,2-Dichloroethane-d4 2.38 2.50 95 75-120 <br /> Surrogate:Toluene-d8 2.48 2.50 99 80-120 <br /> Surrogate:4-Bromofluorobenzene 2.40 2.50 96 60-135 <br /> Laboratory Control Sample(7C30048-BS1) Prepared:03/30/07 Analyzed:03/31/07 <br /> Benzene 10.2 0.50 ug/I 10.0 102 75-120 <br /> Toluene 10.4 0.50 10.0 104 75-120 <br /> Ethylbenzene 10.8 0.50 10.0 108 75-120 <br /> Xylenes(total) 32.0 0.50 30.0 107 75-120. <br /> Methyl tert-butyl ether 10.0 0.50 10.0 100 50-140 <br /> Di-isopropyl ether 10.1 0.50 10.0 101 70-130 <br /> Ethyl tert-butyl ether 10.1 0.50 10.0 101 65-130 <br /> tert-Amyl methyl ether 9.77 0.50 10.0 98 65-135 <br /> tert-Butyl alcohol 188 20 200 94 60-135 <br /> 1,2-Dichloroethane 9.41 0.50 10.0 94 70-125 <br /> 1,2-Dibromoethane(EDB) 9.29 0.50 10.0 93 80-135 <br /> Ethanol 216 100 200 108 15-150 <br /> Surrogate:Dibromofluoromethane 2.50 2.50 100 75-120 <br /> Surrogate:1,2-Dichloroethane-d4 2.39 2.50 96 75-120 <br /> Surrogate:Toluene-d8 2.54 2.50 102 80-120 <br /> Surrogate:4-Bromofluorobenzene 2.60 2.50 104 60-135 <br /> TestAmerica-Sacramento,CA The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document. Unless otherwise stated,results are reported on a wet weight basis. <br /> This analytical report must be reproduced in its entirety. <br /> Page 17 of 23 <br />