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4D Sequoia Morgan�F� i.CA 95037 <br /> (448)77696W <br /> 0''moo Analytical FAX(408)782-6308 <br /> Cambria-Oakland(Shell) Project Shell Sampled 10/25/99 <br /> 1144 65th St Suite C Project Number 341 E Main St.,Ripon Received 10/27/99 <br /> Oakland,CA 94608 Project Mane er Owen Ratch a Reported 11/17/99 <br /> Volatile Organic Oxygenated Compounds by EPA Method 8260A <br /> Sequoia Analytical-San Carlos <br /> Batch Date Date Surrogate Reporting <br /> Anal Number Prepared Analyzed Limits Limit Result Units Notes' <br /> NM-5A-"9 5(continued) M910AAO-10 Soil <br /> Tert-butyl alcohol 9110017 11/3199 1113/99 10 0 ND mg/kg <br /> Methyl tert-butyl ether " " " 0 100 ND " <br /> Di-isopropyl ether 0100 ND " <br /> Ethyl tent-butyl ether 0100 ND " <br /> Tert-amyl methyl ether " _"_ __ 0100 ND <br /> Surrogate 1,2-Dichloroethane-d4 " 70 0-121 T T 104 % � <br /> KW-5A-24 5 91 O-1 1 Soil <br /> Ethanol 9110017 1113199 1113/99 500 ND mg/kg <br /> Tert-butyl alcohol of 100 ND <br /> Methyl tert-butyl ether " 0 100 ND <br /> Da-isopropyl ether 0 100 ND " <br /> Ethyl tert-butyl ether 0 100 ND " <br /> —Tert-amyl methyl ether "_ _ 0100 ND_ " <br /> Mwropte 12-Dichloroethane-d4 " 700-121 912 % <br /> -SA-30 0 M910AAO-12 Sot <br /> Ethanol 9110017 11/3/99 11/3/99 50 0 ND mg/kg <br /> Test b.atyl alcohol to 10 0 ND " <br /> Methyl tent-butyl ether " " " 0100 ND " <br /> Di-isopropyl ether do 0 100 ND " <br /> Ethyl tert-butyl ether " 0 100 ND " <br /> Tert-amyl methyl ether 0 100 ND " <br /> Surrogate 1,2-Dichloroethane-d4 700-121 106 % <br /> MW-SA-34 S M910AAG-13 §211 <br /> Ethanol 9120017 11/3/99 11/3199 500 ND mg/kg <br /> Tert-butyl alcohol too ND " <br /> Methyl tert-butyl ether 0 100 ND It <br /> Da-isopropyl ether " 0 100 ND " <br /> Ethyl tert-butyl ether " 0100 ND " <br /> Tert-am 1 methyl ether " 0100 14D " <br /> Surrogate 1,2-Drchloroethane-d4 " 700-121 836 % <br /> i <br /> uoia Analytical-Morgan Hill 'Refer to end of report for text of notes and definitions <br /> Page 9 of 13 <br />