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1551 Industrial <br /> ad <br /> 4 4D <br /> Sequoia San Carlos CA 94070-4111 <br /> (650) 232-9600 <br /> Analytical <br /> FAX(650) 232-9612 <br /> Blaine Tech Services Project Shell(2) Sampled 5/18/99 <br /> 1680 Rogers Avenue Project Number Shell 341 East Main St,Ripon Received 5/21/99 <br /> San Jose,CA 95112 Project Manager Fran Thie Reported 6/10/99 <br /> 0VTBE-- - Method 8260AIQualityCo trot <br /> d <br /> Sequola Analyttcal�-MSan Carlos ' ' <br /> r� y �W _ _ _ ._ M _ <br /> Date Spike Sample QC Reporting Limit Recov RPD RPD <br /> Ana] Analyzed Level Result Result Units Recov Limits % Limit % Notes* <br /> Batch 9060045 Date Prepared 6/7199 Extraction Method EPA 5030B [P/T) <br /> Blank 9060045-BLK1 <br /> Methyl tert-butyl ether 6/7/99 ND ug/l 200 _ <br /> Surrogate 1,2-Dichloroethane-d4 500 515 760-114 103 <br /> Blank 9060045-BLK2 <br /> _Methyl tert-butyl ether 6/8/99 ND ug/1 200 <br /> Surrogate 1,2-Dichloroethane-d4 500 51 7 Fo 760-114 103 <br /> LCS 9060045-BSI <br /> Methyl tert-butyl ether 6/7/99 500 521 ug/1 700-130 104 <br /> Surrogate 1,2-Dichloroethane-d4 500 511 760-114 102 <br /> LCS 9060045-BS2 <br /> Methyl tert-butyl ether 6/8/99 500 53 8 ug/l 700-130 108 <br /> Wgate 1 2-Dichloroethane-d4 500 530 760-114 106 <br /> Matrix Spike 9060045-MS1 L905542-03 <br /> Methyl tert-butyl ether 6/8/99_ 50 0 ND 638 ug/l 600-140 128 <br /> Surrogate 1,2-Dichloroethane-d4 50 0 56 3 760-114 113 <br /> Matrix Spike Dua 9060045-MSDI L905542-03 <br /> Methyl.ter t-butyl ether 6/8/99 Soo ND 654 ug/1 600-140 131 25 0 2.32 <br /> Surrogate 1,2-Dich1oroethane-d4 500 561 re 760-114 112 <br /> nota Analytical-San Carlos *Refer to end of report for text of notes and definitions <br /> Page 6 of 7 <br />