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Sequoia 1551 1 Road <br /> San Carlos CAA 94070-4111 <br /> 4070 94070_q 1 I 1 <br /> (650) 232-9600 <br /> Analytical <br /> FAX(650) Z32-9612 <br /> m <br /> Blaine Tech Services Project Shell(2) Sampled 6/1/99 <br /> 1680 Rogers Avenue Project Number Shell,990601 Y4,341 East Main St Received 6/2/99 <br /> San Jose,CA 95112 Project Manager Ann Pember Reported 6/21/99 <br /> n r8a t <br /> ty Control <br /> t n3E i �r <br /> s�, <br /> i <br /> ,',Se+ uoxa '€; <br /> 1 3 <br /> ._��..�-�.»e,.:�.,..Y <br /> - - Date - Spike Sample QC Reporting Limit Recov RPD=�% N <br /> Analyte Analyzed Level Result Result Units Recov Limits % Lima <br /> Batch 9060083 Date Prepared 6114/99 Extraction Method EPA 5030B [PIT] <br /> Blank 9060083-BLK1 <br /> Methyl tert-butyl ether 6/14/99 ND ug/l 200 <br /> Surrogate 12-Drchloroethane-d4 500 564 760-114 113 <br /> Blank 9060083-BLK2 <br /> Methyl tent-butyl ether 6/15/99 ND ug/l 200 <br /> Surrogate 1,2-Drchloroethane-d4 500 538 760-114 108 <br /> Blank 9060083-BLK3 <br /> Methyl tert-butyl ether 6/18/99 ND ug/1 200 <br /> Surrogate 1 2-Drchloroethane-d4 01500 509 760-114 102 <br /> GCS 9060083-BSI <br /> Methyl tert-butyl ether 6/14/99 500 543 ug/l 700-130 109 <br /> Surrogate 1,2-Dichloroethane-d4 11 500 55 0 760-114 110 <br /> LCS 9060083-BS2 <br /> Methyl tert-butyl ether 6/15199 500 516 ug/l 700-130 103 <br /> —_.Surrogate–1,2-Dichloroethane-d4 –500 567 76 0-114-- --113 <br /> LCS 9060083-B S3 <br /> Methyl tert-butyl ether 6/18/99 500 540 ug/l 700-130 108 <br /> Surrogate 12-Drchloroethane-d4 11500 510 760-114 102 <br /> Matrix Spike 9060083-MS1 L906220-14 <br /> Methyl tert-butyl ether 6/14/99 500 961 547 ug/l 600-140 902 <br /> Surrogate 1 2-Drchloroethane-d4 " 500 545 760-114 109 <br /> Matrix Spike Dup 9060083-MSDI L906220-14 <br /> Methyl tert-butyl ether 6/14/99 50 0 961 -58 7 ug/l 600-140 982 250. 8 49 <br /> Surrogate 1 2-Dichloroethane-d4 500 539 760-114 108 <br /> Sequoia Analytical-San Carlos *Refer to end of report for text of notes and def nrtror <br /> Page 5 of 6 <br />