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Lancaster <br /> Laboratories Analysis Report <br /> 242$New Holland Pike,PC Box 12425 Lancaster PA 17605 2425•717 656 2300 Fax 717-656-2681•www Iancastertabs com <br /> Page 2 of 5 <br /> Quality Control Summary <br /> Client Name ChevronTexaco Group Number 882407 <br /> Reported 01/30/04 at 12 08 PM <br /> Laboratory Compliance Quality Control <br /> Blank Blank Report LCS LCSD LCS/LCSD <br /> Analysis Name Result ML- Unita %REC %REC Limits RPD RPD Max <br /> Xylene (Total) N D 5 ug/l 90 84-120 <br /> Sample Matrix Quality Control <br /> Ms MSD MS/MSD RPD BKG DUP DUP Dup <br /> RPD <br /> Analysis Name %REC %REC Limits RPD MAX Conc Conc RPD Max <br /> Batch number 040260007A Sample number(s) 4204149-4204151 <br /> Methanol (by Direct Infection) 100 98 73-117 2 20 <br /> Batch number 04027A56A Sample number(s) 4204150 <br /> TPH-GRO - Waters 114 63-154 <br /> Batch number 04028A07B Sample number(s) 4204151-4204152 <br /> TPH-GRO - Waters 99 101 63-154 2 30 <br /> Batch number 04029A07A Sample number(B) 4204148 <br /> TPH-GRO - Waters 103 101 63-154 1 30 <br /> Batch number 04029A07B Sample numbers) 4204149 <br /> TPH-GRO - Waters 103 141 63-154 1 30 <br /> Batch number P040262AA Sample number(s) 4204148 <br /> Methyl Tertiary Butyl Ether 98 99 69-134 1 30 <br /> Benzene 103 118 63-128 12 30 <br /> Toluene 103 115 83-127 10 30 <br /> Ethylbenzene 103 110 82-129 6 30 <br /> Xylene (Total) 104 137* 82-130 22 30 <br /> Batch number P040272AA Sample number(s) 4204152 <br /> Methyl Tertiary Butyl Ether 101 101 69-134 1 30 <br /> di-Isopropyl ether 106 107 75-130 1 30 <br /> Ethyl t-butyl ether 102 103 78-119 1 30 <br /> t-Amyl methyl ether 98 100 77-117 2 30 <br /> t-Butyl alcohol 106 109 51-147 3 30 <br /> Benzene 104 105 83-128 1 30 <br /> Toluene 103 104 83-127 1 30 <br /> Ethylbenzene 104 106 82-129 2 30 <br /> Xylene (Total) 103 105 82-130 1 30 <br /> Batch number P040291AA Sample number(s) 4204149-4204150 <br /> Ethanol 113 124 41-155 9 30 <br /> Methyl Tertiary Butyl Ether 97 97 69-134 0 30 <br /> di-Isopropyl ether 108 106 75-130 2 30 <br /> Ethyl t-butyl ether 104 104 78-119 1 30 <br /> t-Amyl methyl ether 101 97 77-117 4 30 <br /> t-Butyl alcohol 107 105 51-147 2 30 <br /> Benzene 102 99 83-128 3 30 <br /> Toluene 101 98 83-127 3 30 <br /> Ethylbenzene 100 99 82-129 1 30 <br /> Xylene (Total) 99 97 82-130 2 30 <br /> Batch number P040292AA Sample number(s) 4204151 <br /> Ethanol 94 88 41-155 8 30 <br /> *-Outside of specification <br /> (1) The result for one or both determinations was less than five times the LOQ <br /> (2) The background result was more than four times the spike added <br />