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Lancaster <br /> Laboratories Analysis Report <br /> 2425 New Holland Pike PO Box 12425 Lancaster,PA 17605.2425•717-656 2300 Fax 717 656-2681•www lancasterlabs com <br /> Page 4 of 5 <br /> Quality Control Summary <br /> Client Name ChevronTexaco Group Number 882407 <br /> Reported 01/30/04 at 12 06 PM <br /> Surrogate Quality Control <br /> Batch number 04029A07A <br /> Trifluorotoluene-F <br /> 4204148 77 <br /> Blank 78 <br /> LCS 99 <br /> MS 117 <br /> MSD 116 <br /> Limits 57-146 <br /> Analysis Name TPH-GRO - Waters <br /> Batch number 04029A07B <br /> Trifluorotoluene-F <br /> 4204149 79 <br /> Blank 77 <br /> LCS 99 <br /> MS 117 <br /> MSD 116 <br /> Limits 57-146 <br /> Analysis Name BTEX+MTBE by 8260B <br /> Batch number P040262AA . <br /> Dibromofluoromethane 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene <br /> 4204148 103 104 105 102 <br /> Blank 104 104 105 101 <br /> LCS 103 102 105 102 <br /> MS 105 105 105 101 <br /> MSD 105 104 104 103 <br /> Limits 81-120 82-112 85-112 83-113 <br /> Analysis Name BTEX+5 Oxygenates by 8260E <br /> Batch number P040272AA <br /> Dibromofluoromethane 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene <br /> 4204152 103 105 105 102 <br /> Blank 104 105 104 101 <br /> LCS 104 105 104 103 <br /> MS 104 106 104 103 <br /> MSD 105 106 105 103 <br /> Limits 81-120 82-112 85-112 83-113 <br /> Analysis Name BTEx+5 Oxygenates+ETOH <br /> Batch number P040291AA <br /> Dibromofluoromethane 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene <br /> 4204149 97 97 95 95 <br /> 4204150 97 97 95 95 <br /> Blank 96 96 95 94 <br /> LCS 96 96 95 95 <br /> MS 97 97 96 95 <br /> MSD 96 97 95 96 <br /> Limits 81-120 82-112 85-112 83-113 <br /> *-Outside of specification <br /> (1) The result for one or both determinations was less than five times the LOQ <br /> (2) The background result was more than four times the spike added 0 <br />