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1 1 II <br /> 885 Jarvis Drive <br /> Sequoia Morgan Hill CA 95037 <br /> (408)776 9600 <br /> Analytical <br /> FAX( )782-6308 <br /> %v%kw sequoialabs cam <br /> Blame Tech Services(Shell) Project ect 1071 North Main Street <br /> 1680 Rogers Avenue Project Number 1071 North Main Street/Manteca Reported <br /> San Jose CA,95112 Project Manager Nick Sudano 09/25/00 15 50 <br /> Volatile Organic Compounds by EPA Method 8260A - Quali_ty Control <br /> Sequoia Analytical - Morgan Hill <br /> Reporting Spike Source %REC RP=Nt,,Analyte Result Limit Units Level Result %REC Limits RPD Lim <br /> Batch OH11012 -EPA 503 OB [PIT] <br /> Blank(OH11012-BLKI) _ _Prepared&Analyzed-08/1-0/00— <br /> Ethanol <br /> nalyzed08/10/00Ethanol ND 400 ug/l <br /> tert-Butyl alcohol ND 200 " <br /> Methyl cert-butyl ether ND 1 00 " <br /> Di-isopropyl ether ND 100 " <br /> Ethyl tert-butyl ether ND 1 00 <br /> tert-Amyl methyl ether ND 100 " <br /> 1,2-Dichloroethane ND 100 " <br /> Ethylene dibrornide ND 1 00 <br /> Surrogate 11-Dichloroethane-d4 110 100 T 110 70-130 _ <br /> LCS(OHI 1012-BS1) J - - — _ Prepared_&Analyzed 08/10/00----- <br /> Methyl <br /> 8/10/00___ _Methyl tent-butyl ether _ 103 too ug/l 100 103 70-130 <br /> Surrogate 11-Dtchloroethane-d4 113 100 113 70-130 <br /> Matrix Spike(OH11012-MS1)_ _ Source MJG0838-01 Prepared 08/10/00 Analyzed 08/11/00 <br /> Methyl tett-butyl ether 529 20 0—ug/1-200-337-96 070=130 <br /> Surrogate 1 2-Dtchloroethane-d4 _—---- 112 �--- "-—--IO 0 ----� 111 70-130 <br /> Matnx Spike Dup(OHI 1012-MSD1) ___Y Source MJG0838-001� Prepared 08/10/00 Analyzed 08/11/00 <br /> Methyl ten-butyl ether 533 200 ug/l 200 337 980 70-130 0 753 25 <br /> Surrogate I 1-Dichloroethane-d4 �v 114 -" 100 114 70-130 <br /> Batch OH12001 -EPA 5030B IP/T] <br /> Blank(OH12001-BLKI) _ Prepared&Analyzed 0811 I/00 _ <br /> Ethanol ND 400 up/l <br /> tert-Butyl alcohol ND 200 " <br /> Methyl tert-butyl ether ND 1 00 <br /> Di-isopropyl ether ND too <br /> Ethyl tert-butyl ether ND 1 00 <br /> tert-Amyl methyl ether ND 100 <br /> I2-Dichloroethane ND 100 " <br /> Ethylene dibromide ND 100 " <br /> Surrogate 1 2-Dichloroethane-d4 101 100 101 70 130 <br /> Sequoia Analytical- Morgan Hill The results in this report apply to the samples analyzed in accordance with the c1 <br /> custody document This analytical report must be reproduced in its entirety <br /> Page 10 of 17 <br />