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Report Number: 86254 <br /> Date : 10/17/2013 <br /> QC Report : Matrix Spike/ Matrix Spike Duplicate <br /> Project Name : Huntbrook Holdings- Stockton <br /> Project Number: <br /> Spiked <br /> Duplicate Spiked Spiked to Sample Relative <br /> Spike Spiked Spiked Sample Sample Relative Percent Percent <br /> iked Sample Spike Dup. Sample Sample Analysis Date Percent Percent Percent Recov. Diff. <br /> Parameter Sapmple Value Level Level Value Value Units Method Analyzed Recov. Recov. Diff. Limit Limit <br /> S <br /> TPH as Diesel <br /> 86254-01 <1.0 19.9 19.7 19.7 19.6 mg/Kg M EPA 8015 10/15/13 99.3 99.8 0.476 60-140 25 <br /> TPH-D (Si Gel) <br /> 86254-01 <1.0 19.9 19.7 22.1 21.7 mg/Kg M EPA 8015 10/15/13 111 110 0.989 60-140 25 <br /> TPH as Diesel <br /> 86281-01 1.6 19.5 19.9 20.0 21.2 mg/Kg M EPA 8015 10/16/13 94.2 98.1 4.07 60-140 25 <br /> TPH-D (Si Gel) <br /> 86281-01 1.2 19.5 19.9 21.9 23.1 mg/Kg M EPA 8015 10/17/13 106 110 3.52 60-140 25 <br /> 1,1,1,2-Tetrachloroethane <br /> 86254-01 <0.0050 0.0397 0.0396 0.0388 0.0372 mg/Kg EPA 8260B 10/15/13 97.7 93.9 3.93 70.0-130 25 <br /> 1,1,1-Trichloroethane <br /> 86254-01 <0.0050 0.0397 0.0396 0.0339 0.0322 mg/Kg EPA 82608 10/15/13 85.3 81.2 4.90 70.0-130 25 <br /> 1,1,2,2-Tetrachloroethane <br /> 86254-01 <0.0050 0.0397 0.0396 0.0423 0.0400 mg/Kg EPA 82608 10/15/13 107 101 5.39 70.0-130 25 <br /> 1,1,2-Trichloroethane <br /> 86254-01 <0.0050 0.0397 0.0396 0.0392 0.0378 mg/Kg EPA 82606 10/15/13 98.8 95.5 3.40 70.0-130 25 <br /> 1,1-Dichloroethane <br /> 86254-01 <0.0050 0.0397 0.0396 0.0343 0.0325 mg/Kg EPA 8260B 10/15/13 86.5 82.0 5.25 70.0-130 25 <br /> w <br /> m <br /> m <br /> w <br /> w <br /> 0 <br /> A <br /> KIFF ANALYTICAL, LLC <br /> 2795 2nd Street, Suite 300 Davis, CA 95618 530-297-4800 <br />