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Entech Analytical Labs, Inc. <br /> 3334 Victor Court - Santa Clara, CA 95054 a (408) 588-0200 - Fax (408) 588-0201 <br /> Compliance&Closure,Inc Date 12/12/00 <br /> 7020 Koll Center Parkway,Suite 134 Date Received 12/1/00 <br /> Pleasanton,CA 94566-3107 Project Name Quick Stop#121 <br /> Project Number 12118-5 <br /> Attu Gary Mulkey P O Number <br /> Sampled By Gary R Mulkey <br /> Certified Analytical Report <br /> Order ID 23405 Lab Sample ID 23405-002 Client Sample ID MW-4-10 <br /> Sample Time- 8 55 AM Sample Date 11/29/00 Matrix Solid <br /> Parameter Result Flag DF PQL DLR Units Analysis Date QC Batch ID Method <br /> Dusopropyl Ether ND 1 5 5 pg/Kg 12/6/00 SMS2001205 EPA 8260B <br /> Ethyl-t-butyl Ether ND 1 5 5 pg/Kg 1216/00 SMS2001205 EPA 82608 <br /> Methyl-t-butyl Ether 180 1 5 5 µg/Kg 12/6/00 SMS2001205 EPA 8260B <br /> tert-Amyl Methyl Ether ND 1 5 5 pg/Kg 12/6/00 SMS2001205 EPA 8260B <br /> tent-Butanol 630 1 20 20 pg/Kg 12/6/00 SMS2001205 EPA 8260B <br /> Surrogate Surrogate Recovery Control Limits(%) <br /> 4-Bromofluorobenzene 102 65 - 135 <br /> Dibromofluoromethane 112 65 - 135 <br /> Toluene-d8 99 65 - 135 <br /> DF=Dilution Factor ND=Not Detected DLR=Detection Umit Reported PQL—Practical Quantitation Limit <br /> Analysis performed by Entech Analytical Labs,Inc (CA ELAP#2346) <br /> -- 12 --� Environmental Analysis Since 7983 <br /> Miche a Anderson, Laboratory Director Page 2 o f 6 <br />