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I <br /> .�I <br /> J <br /> Lancaster , - , . <br /> Laboratories Analysis Report <br /> 2425 New Holland Pike,PO Box 12425,Lancaster,PA 17605.2425•717-656-2300 Fax:717-656-2681•www.lancasterlabs.com <br /> Page 2 of 3 <br /> Quality Control Summary s <br /> Client Name: ChevronTexaco Group Number: 917560 <br /> Reported: 11/03/01 at 04:53 PM <br /> Sample Matrix Quality Control <br /> M5 MSD MS/MSD RPD BKG DUP DUP Dup APD <br /> Analysis Name goREC 9oREC Limits RPD MAX Cone - Cone RPD Max <br /> di-Isopropyl ether 95 100 75-130 5 30 <br /> Ethyl t-butyl ether 93 99 78-119 ' 6 30 ¢ <br /> t-Amyl methyl ether 91 97 77-117 6 30 <br /> t-Butyl alcohol 89 93 51-147 4 30 <br /> Benzene 98 105 83-128 7 30 <br /> 1,2-Dichloroethane 95 101 73-136 6 30 <br /> Toluene 99 106 83--127 7 30 <br /> 1,2-Dibromoethane 91 96 78-120 6 30 <br /> Ethylbenzene 100 106 82-129 5 30 <br /> Xylene (Total) 97 102 82-130 6 30 <br /> Batch number: Z043071AA Sample number(s) : 4385470 <br /> Ethanol 80 86 33-153 7 30 t^ <br /> Methyl Tertiary Butyl Ether 93 99 69-134 5 30 ' <br /> di-Isopropyl ether 99 104 75-130 5 30 <br /> Ethyl t-butyl ether 96 101 78-119 5 30 <br /> t-Amyl methyl ether 92 97 77-117 5 30 <br /> t-Butyl alcohol 91 93 51-141 2 30 <br /> Benzene 100 105 83-128 5 30 <br /> 1,2-Dichloroethane 101 104 73-136 2 30 ; <br /> Toluene 104 106 83-127 2 30 <br /> 1,2-Dibromoethane 94 97 78-120 3 30 <br /> Ethylbenzene 102 106 82-129 4 30 <br /> Xylene (Total) 99 102 82-130 3 30 <br /> Surrogate Quality Control <br /> Analysis Name: TPH-GRo - waters <br /> Batch number: 04299A08E <br /> Trifluorotoluene-F <br /> w <br /> 4385470 100 <br /> 4385471 102 <br /> 4385472 100 <br /> 4385473 102 <br /> Blank 101 <br /> LCS 117 <br /> LCSD 110 <br /> MS 100 #` <br /> Limits: 57-146 ! <br /> Analysis Name: BTEX+5 0xygenates+EDC+EDB+ET0H <br /> Batch number: 2043061AA <br /> Dibromofluoromethane 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene <br /> 4385471 92 94 98 92 <br /> 4385472 92 93 96 93 <br /> 4385473 91 93 98 93 <br /> Blank 93 91 98 93 <br /> LCS 93 93 97 95 <br /> MS 53 93 98 96 <br /> *-Outside of specification <br /> (1) The result for one or both determinations was less than five times the LOQ. <br /> (2) The background result was more than four times the spike added. <br /> 'IJ <br />