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Lancaster <br /> Laboratories Analysis Report <br /> 2425 Now Holland Pike PO Bax 12425 Lancaster PA 176052425•717 656 2300 Fax 717 656-2681•www lancasterlabs com <br /> Page 3 of 3 <br /> Quality Control Summary <br /> Client Name ChevronTexaco Group Number 885277 <br /> Reported 02/27/04 at 01 56 PM <br /> Surrogate Quality Control <br /> Limits 57-146 <br /> Analysis Name BTEX+S Oxygenates+EDC+EDB+ETOH <br /> Batch number P049553AA <br /> Dibromofluoromethane 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene <br /> 4219187 98 97 100 97 <br /> Blank 97 97 100 96 <br /> LCS 98 96 100 97 <br /> MS 98 96 100 96 <br /> MSD 97 95 99 96 <br /> Limits 81-120 82-112 85-112 83-113 <br /> Analysis Name BTEX+5 Oxygenates+EDC+EDB+ETOH <br /> Batch number P040561AA <br /> Dibromofluoromethane 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene <br /> 4219188 97 95 99 96 <br /> 4219189 99 95 99 95 <br /> Blank 96 96 99 95 <br /> LCS 97 96 99 96 <br /> MS 96 94 99 95 <br /> MSD 98 97 98 95 <br /> Limits 81-120 82-112 85-112 83-113 <br /> Analysis Name 8260 Master Scan (water) <br /> Batch number P040571AA <br /> Dibromofluoromethane 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene <br /> Blank 97 94 99 96 <br /> LCS 98 95 99 96 <br /> MS 98 96 98 95 <br /> MSD 99 96 99 97 <br /> Limits 81-120 82-112 85-112 83-113 <br /> *-Outside of specification <br /> (1) The result for one or both determinations was less than five times the LOQ <br /> (2) The background result was more than four times the spike added <br />