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I <br /> Lancaster, <br /> Analysis <br /> . Laboratori0es <br /> 5 Report <br /> New Holland Pike PO Box 12425 Lancaster,PA 17605.2425.717 656 2300 Fax 717-656-2681•www Eancasterlabs coal <br /> Pagel of 2 <br /> Lancaster Laboratories Sample No. WW 4165118 <br /> MW-6S-W-031111 Grab Water <br /> Facility# 91452 Job# 386582 GRD <br /> 334 8 Main St Ripon T0607700554 MW-6S <br /> Collected 11/11/2003 11 19 by AS Account Number 10906 <br /> Submitted 11/14/2003 09 35 ChevronTexaco <br /> Reported 11/26/2003 at 15 44 6001 Bollinger Canyon Rd L4310 <br /> Discard 12/27/2003 San Ramon CA 94583 <br /> 3346S <br /> As Received <br /> CAT As Received Method Dilution <br /> No Analysis Name CAS Number Result Detection Units Factor <br /> Limit <br /> 01728 TPH-GRO - Waters n a 3,500 250 ug/l 5 <br /> The reported concentration of TPH-GRO does not include MTBE or other <br /> gasoline constituents eluting prior to the C6 (n-hexane) TPH-GRO range <br /> start time <br /> A sate-specific MSD sample was not submitted for the pro3ect A LCS/LCSD <br /> was performed to demonstrate precision and accuracy at a batch level <br /> 01412 Methanol and Ethanol <br /> 01414 Methanol (by Direct In3ection) 67-56-1 N D 1,000 ug/1 1 <br /> 01594 BTEx+5 Oxygenates+EDC+EDB+ETOH <br /> 01587 Ethanol 64-17-5 N D # 1,300 ug/l 25 <br /> 02010 Methyl Tertiary Butyl Ether 1634-04-4 35,000 130 ug/l 250 <br /> 02011 di-Isopropyl ether 108-20-3 N D # 13 ug/l 25 <br /> 02013 Ethyl t-butyl ether 637-92-3 N D # 13 ug/l 25 <br /> 02014 t-Amyl methyl ether 994-05-8 2,300 13 ug/l 25 <br /> 0201$ t-Butyl alcohol 75-65-0 1,200 130 ug/l 25 <br /> 05401 Benzene 71-43-2 N D # 13 ug/l 25 <br /> 05402 1,2-Dichloroethane 107-06-2 N D # 13 ug/1 25 <br /> 05407 Toluene 108-88-3 N D # 13 ug/l 25 <br /> 05412 1,2-Dibromoethane 106-93-4 N D # 13 ug/l 25 <br /> 05415 Ethylbenzene 100-41-4 N D # 13 ug/l 25 <br /> 06310 xylene (Total) 1330-20-7 N D # 13 ug/l 25 <br /> The reporting limits for the GC/MS volatile compounds were raised <br /> because sample dilution was necessary to bring target compounds into the <br /> calibration range of the system <br /> State of California Lab Certification No 2116 <br /> Laboratory Chronicle <br /> CAT Analysis Dilution <br /> No Analysis Name Method Trial# Date and Time Analyst Factor <br /> 01728 TPH-GRO - Waters N CA LUFT Gasoline 1 11/18/2003 01 43 Martha L Seidel 5 <br /> Method <br /> 1412 Methanol and Ethanol SW-846 8015B 1 11/19/2003 13 31 Tiffany A George 1 <br /> 594 STEX+5 SW-846 8260B 1 11/18/2003 22 01 Elizabeth M Taylor 25 <br /> oxygenates+EDC+EDB+ETOH <br /> #Laboratory MethodDetection Limit exceeded target detection limit <br /> N D=Not detected at or above the Reporting Limit <br />