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Lancaster <br /> Laboratories Analysis Report <br /> 41425'wNe—w Holtand Pike,PO Box 12425 Lancaster,PA 17605-2425•717-656 2300 Fax 717 656-2681•www lancasterlabs coal <br /> Page ] of 2 <br /> Lancaster Laboratories Sample No. WW 4103055 <br /> Collected 08/11/2003 14 25 by JH Account Number 10906 <br /> Submitted 08/15/2003 09 20 ChevronTexaco <br /> Reported 08/27/2003 at 16 54 6001 Bollinger Canyon Rd L4310 <br /> Discard 09/27/2003 <br /> MW-1-W-030811 Grab Water San Ramon CA 94583 <br /> Facility# 91452 Job# 386582 GRD <br /> 334 E Main St Ripon T0607700554 MW-1 <br /> 554-1 <br /> As Received <br /> CAT As Received Method Dilution <br /> No Analysis Name CAS Number Result Detection Units Factor <br /> Limit <br /> 01728 TPH-GRO - Waters n a N D 50 ug/l 1 <br /> The reported concentration of TPH-GRO does not include MTBE or other <br /> gasoline constituents eluting prior to the C6 (n-hexane) TPH-GRO range <br /> start time <br /> A site-specific MSD sample was not submitted for the project A LCS/LCSD <br /> was performed to demonstrate precision and accuracy at a batch level <br /> 01412 Methanol and Ethanol <br /> 01414 Methanol (by Direct Infection) 67-56-1 N D 1,000 ug/l 1 <br /> 01594 BTEX+5 Oxygenates+EDC+EDB+ETOH <br /> 01587 Ethanol 64-17-5 N D 500 ug/l 1 <br /> 02010 Methyl Tertiary Butyl Ether 1634-04-4 N D 2 — ug/l 1 <br /> 02011 di-Isopropyl ether 108-20-3 N D 2 ug/l 1 <br /> 02013 Ethyl t-butyl ether 637-92-3 N D 2 ug/l 1 <br /> 02014 t-Amyl methyl ether 994-05-8 N D 2 ug/l 1 <br /> 02015 t-Butyl alcohol 75-65-0 N D 100 ug/l 1 <br /> 05401 Benzene 71-43-2 N D 0 5 ug/l 1 <br /> 05402 1,2-Dichloroethane 107-06-2 N D 2 ug/l 1 <br /> 05407 Toluene 108-88-3 N D 0 5 ug/l 1 <br /> 05412 1,2-Dibromoethane 106-93-4 N D 2 ug/l 1 <br /> 05415 Ethylbenzene 100-41-4 N D 0 5 ug/l 1 <br /> 06310 Xylene (Total) 1330-20-7 N D 0 5 ug/1 1 <br /> State of California Lab Certification No 2116 <br /> Laboratory Chronicle <br /> CAT Analysis Dilution <br /> No Analysis Name Method Trial# Date and Time Analyst Factor <br /> 01728 TPH-GRO - Waters N CA LUFT Gasoline 1 08/19/2003 12 12 K Robert Caulfeild- 1 <br /> Method ,lames <br /> 01412 Methanol and Ethanol SW-846 8015B 1 08/21/2003 12 23 Lisa A Johnson 1 <br /> 01594 STEX+5 SW-846 8260B 1 08/20/2003 17 01 Trent S Sprenkle 1 <br /> Oxygenates+EDC+EDB+ETOH <br /> 146 GC VOA Water Prep SW-846 5030E 1 08/19/2003 12 12 K Robert Caulfeild- n a <br /> James <br /> 0,163 GC/MS VOA Water Prep SW-846 5030B 1 08/20/2003 17 01 Trent S Sprenkle n a <br /> #=Laboratory MethodDetection Limit exceeded target detection hm1t <br /> N D=Not detected at or above the Reporting Limit <br />