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Lancaster <br /> Laboratories Analysis Rep art <br /> 25 New Holland Pike,PO Box 12425 Lancaster,PR 17605-2425+717-656 2300 Fax 717 656-2681+www lancasterlabs eom <br /> Page 1 of 2 <br /> Lancaster Laboratories Sample No. Ww 4103061 <br /> Collected 08/11/2003 10 50 by JH Account Number 10906 <br /> Submitted 08/15/2003 09 20 ChevronTexaco <br /> Reported 08/27/2003 at 16 55 6001 Bollinger Canyon Rd L4310 <br /> Discard 09/27/2003 <br /> MW-6S-W-030811 Grab Water San Ramon CA 94583 <br /> Facility# 91452 Job# 386582 GRD <br /> 334 E Main St Ripon 70607700554 MW-6S <br /> 5546S <br /> As Received <br /> CAT As Received Method Dilution <br /> No Analysis Name CAS Number Result Detection Unita Factor <br /> Limit <br /> 01728 TPH-GRO - Waters n a 2,200 250 ug/l 5 <br /> The reported concentration of TPH-GRO does not include MTBE or other ` <br /> gasoline constituents eluting prior to the C6 (n-hexane) TPH-GPO range <br /> Start time <br /> A site-specific MSD Sample was not submitted for the pro3ect A LCS/LCSD <br /> was performed to demonstrate precision and accuracy at a batch level I <br /> 01412 Methanol and Ethanol <br /> 01414 Methanol (by Direct In3ection) 67-56-1 N D 1,000 ug/1 1 <br /> 01594 BTEX+5 Oxygenates+EDC+EDB+ETOH <br /> 01587 Ethanol 64-17-5 N D # 2,000 ug/l 40 <br /> 02010 Methyl Tertiary Butyl Ether 1634-04-4 31,000 200 ug/1 400 <br /> 02011 di-Isopropyl ether 108-20-3 N D # 20 ug/1 40 <br /> 02013 Ethyl t-butyl ether 637-92-3 N D # 20 ug/1 40 <br /> 02014 t-Amyl methyl ether 994-05-8 1,900 20 ug/l 40 <br /> 02015 t-Butyl alcohol 75-65-0 3,000 200 ug/1 40 <br /> 05401 Benzene 71-43-2 N D # 20 ug/1 40 <br /> 05402 1,2-Dichloroethane 107-06-2 N D # 20 ug/1 40 <br /> 05407 Toluene 106-88-3 N D # 20 ug/1 40 <br /> 05412 1,2-Dibromoethane 106-93-4 N D # 20 ug/1 40 <br /> 05415 Ethylbenzene 100-41-4 N D # 20 ug/1 40 <br /> 06310 Xylene (Total) 1330-20-7 N D # 20 ug/1 40 <br /> The reporting limits for the GC/MS volatile compounds were raised <br /> because sample dilution was necessary to bring target compounds into the <br /> calibration range of the system <br /> Stage of California Lab Certification No 2116 <br /> Laboratory Chronicle <br /> CAT Analysis Dilution <br /> No Analysis Name Method Trial# Date and Time Analyst Factor <br /> 01728 TPH-GRO - Waters N CA LUFT Gasoline 1 08/19/2003 15 46 K Robert Caulfeild- 5 <br /> Method James <br /> 412 Methanol and Ethanol SW-846 8015B 1 08/21/2003 14 20 Lisa A Johnson 1 <br /> 594 BTEX+5 SW-846 8260E 1 08/23/2003 01 12 Elizabeth M Taylor 40 <br /> Oxygenates+EDC+EDB+ETON <br /> #=Laboratory MethodDetection Limit exceeded target detection limit <br /> N D=Not detected at or above the Reporting Limit <br />