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Lancaster <br /> r Laboratories Analysis Report ., <br /> 2425 New Holland Pike PO Box 12425 Lancaster PA 17605.2425-717656-2300 Fax 717-656-2681•www Iancasterlabs Com <br /> Page 4 of 4 <br /> Quality Control Summary <br /> Client Name ChevronTexaco Group Number 850838 <br /> Reported 05/19/03 at 07 36 AM <br /> Surrogate Quality Control <br /> Ms 105 <br /> MSD 107 <br /> Limits 57-146 <br /> Analysis Name BTEX + Oxygenates by 8260B <br /> Batch number N031322AB <br /> Dibromofluoromethane 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene <br /> 4039135 97 100 98 90 <br /> 4039136 97 99 97 89 <br /> 4039137 97 99 97 69 <br /> 4039138 98 100 97 89 <br /> 4039139 97 98 97 89 <br /> 4039140 95 98 98 91 <br /> 4039141 96 98 98 90 <br /> 4039142 95 100 98 89 <br /> 4039143 97 100 96 88 <br /> Blank 97 99 97 91 <br /> LCS 98 102 96 96 <br /> MS 98 302 95 97 <br /> MSD 97 101 96 97 <br /> Limits 81-120 82-112 85-112 83-113 <br /> Analysis Name BTEX + Oxygenates by 8260B • <br /> Batch number N031351AA <br /> Dibromofluoromethane 1,2-Dichloroethane-d4 Toluene-dB 4-Bromofluorobenzene <br /> 4039144 97 99 96 89 <br /> 4039145 94 99 96 90 <br /> Blank 97 101 97 90 <br /> LCS 95 98 98 94 <br /> MS 96 99 98 95 <br /> MSD 95 99 98 95 <br /> Limits 81-120 82-112 85-112 83-113 <br /> *-Outside of specification <br /> (l) The result for one or both determinations was less than five times the LOQ - <br /> (2) The background result was more than four times the spike added <br />