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110 2nd Avenue South,#D7,Pacheco,CA 94553 <br /> McCAMPBELL ANALYTICAL INC. Tele:510-798-1620 Fax:510-798-1622 <br /> Advanced GeoEnvironntental Client Project ID:Exxon Station Date Sampled:06/06/95 <br /> 1803 West March Lane,Ste.A Date Received:06/07/95 <br /> Stockton,CA 95207 Client Contact:Bob Marty/Mike Flores Date Extracted:06/07-06-22/95 <br /> Client P.O: Date Analyzed:06/08&06/22/95 <br /> LUFT Metals <br /> EPA anal ical methods 6010/200.7 239.2' <br /> Rec. <br /> Lab ID Client ID Matrix Extraction° Cadmium Chromium Lead Nickel Zinc Surrogate <br /> 53155 Tank 4 PB 8' S TTLC ND 39 21 33 53 103 <br /> 53156 Tank 4 SP S TTLC ND 34 130 36 94 102 <br /> 53155 Tank 4 PB 8' S STLC — 0.71 1.2 0.90 5.6 NA <br /> 53156 Tank 4 SP S STLC — 0.15 11 0.58 8.1 NA <br /> Reporting Limit unless other- s TTLC 0.5 mg/L 0.5 3.0 2.0 1.0 <br /> wise stated;ND means not de- <br /> tected show the reporting limit W TTLC 0.01 mg/kg 0.005 0.005 0.02 0.01 <br /> STLC,TCLP 0.01 mg/L 0.05 0.2 0.05 0.05 <br /> "soil samples are reported in mg/kg,and water samples and all STLC&TCLP extracts in mg/L <br /> + Lead is analysed using EPA method 6010(ICP)for soils,STLC&TCLP etlracts and method 239.2(AA Furnace)for water samples <br /> o EPA etaraction methods 1311(TCLP),3010/3020(water,TTLC),3040(organic matrices -MC),30Wsolids,TTLC);STLC from CA Title <br /> 22 <br /> # surrogate diluted out of range;N/A means surrogate not applicable to this analysis <br /> i) liquid sample that contains greater than — 2 vol. % sediment;this sediment is extracted with the liquid, in accordance with EPA <br /> methodologies and can significantly effect reported metal concentrations. <br /> DHS Certification No. 1644 <br /> Edward Hamilton-Lab Director <br />