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To Tom Ballard From Sparger Technology 362-0947 Thu 25 Apr 2002 16 07 42 Page 4 <br /> Analytical Laboratory Division <br /> Spargero Mobile Laboratory Division <br /> . Techhobgy, Scientific Division <br /> Test Certificate of Analysis <br /> Client ID G H H Engmeenng Workorder ID 518710 JAMAR <br /> Workorder If 14653 Sampled 04/17/02 <br /> Laboratory ID 14653003 Received 04/18/02 <br /> Sample ID MW-3 Reported 04/25/02 <br /> Matrix Water <br /> 8260B Oxygenates -8260B <br /> Parameter Prep Date Analyzed Result RL Units Dilution <br /> Tertiary butanol 04/23/02 04123102 ND 500 ug/L 1 100 <br /> Methyl--tent-butyl-ether 04/23/02 04/23/02 ND 50 ug/L 1 100 <br /> Di-isopropyl ether 04/23/02 04/23/02 ND 500 ug/L 1 100 <br /> Ethyl tert-butyl ether 04/23/02 04/23/02 ND SOO ug/L 1 100 <br /> Tertiaryamyl methylether 04/23/02 04/23/02 ND 500 ug/L 1 100 <br /> 1,2-DCA 04/23/02 04/23/02 ND 200 ug/L 1 100 <br /> Benzene 04/23/02 04/23/02 14000 50.0 ug/L 1:100 <br /> Toluene 04/23/02 04/23/02 550 50.0 ug/L 1:100 <br /> Ethylbenzene 04/23/02 04/23/02 110 50.0 ug/L 1:100 <br /> Xylene (Total) 04123/02 04/23/02 980 50.0 ug/L 1:100 <br /> • Surrogates Result Recovery Limits <br /> D3.bromodifluoromethane 52 4 ug/L 105 % (76 - 135) <br /> C rUicahon No 1614 Q�j ry`Page 4 of 26 j1 <br />