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I 10 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> 4 McCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax:925-798-1622 <br /> htip://www.mccampbcll.com E-mail: main@mccampbell.com <br /> John P. Cummings&Associates Client Project ID: #0399002.03;Jamar Date Sampled: 08/21/2000 <br /> P.O. Box 2847 Date Received: 08/23/2000 <br /> Fremont, CA 94536-2847 Client Contact: John Cummings Date Extracted: 08123-08131/2000 <br /> Client P.O: Date Analyzed: 08/24-09/01/2000 <br /> Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br /> Lab ID 45645 45646 45647 45648 <br /> Reporting Limit <br /> Client ID B-1 65' B-1 70'. B-1 75' 13-1 80' <br /> Matrix S S S S S W <br /> Compound Concentration* ug/kg ug/L <br /> Di-isopropyl Ether(D1PE) ND<35 ND<25 ND<I5 ND<8.5 5.0 1.0 <br /> Ethyl tert-Butyl Ether(ETBE) ND<35 ND<25 ND<15 ND<8.5 510 1.0 <br /> Methyl-tert Butyl Ethcr(MTBE) 730 700 140 ND<17 5.0 1.0 <br /> tert-Amyl Methyl Ether(TAME) ND<35 ND<25 ND<15 ND<8.5 5.0 1.0 <br /> tent-Butanol ND<180 N0<10 ND<75 ND<43 25 5.0 <br /> Surrogate Recoveries{%) <br /> Dibromolluoromethane 95 89 88 83 <br /> Comments: <br /> *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP I STLC/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit;NIA means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present;(i)liquid sample that contains greater than—5 vol.%sediment;6)sample diluted due to <br /> high organic content <br /> DHS Certification No. 1644 Edward Hamilton,Lab Director <br /> ' I <br />