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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax:925-798-1622 <br /> httoa/www.mccarrrpbell.com E-mail:main@mccampbell.com <br /> John P. Cummings&Associates Client Project ID:#0399002.00;Jamar Date Sampled: 09/08/99 <br /> P.O.Box 2847 SS Date Received:09/13/99 <br /> Fremont,CA 94536-2847 Client Contact: John Cummings Date Extracted: 09/13/99 <br /> Client P.O: Date Analyzed: 09/14-09/16/99 <br /> Diesel Range(C10-C23)Extractable Hydrocarbons as Diesel <br /> EPA methods modified 8015,and 3550 or 3510;Cal ifomia RWQCB(SF Bay Region)method GCFID(3550)or GCFID(3510) <br /> Lab ID Client ID Matrix TPH(dr %Recovery <br /> Surrogate <br /> 19087 B1-15 S ND 107 <br /> 19088 81-20 S 2.0,d 100 <br /> 19089 B 1-25 S 44,d,b 98 <br /> 19090 B1-30 S 42,d,b 105 <br /> 19091 B1-35 S 190,d,b 100 <br /> 19092 B1-40 S 85,d,b 106 <br /> 19093 13145 S 170,d,b 107 <br /> 19094 BI-50 S 690,d 99 <br /> 19095 B1-55 S 140,d,b 100 <br /> 19096 B1-60 S 54,d,b 100 <br /> 19097 BI-65 S 2.2,d 107 <br /> 19098 B1-70 S ND 105 <br /> 19099 Bi-75 S ND 108 <br /> 19100 )31-78 S ND 97 <br /> Reporting Limit unless otherwise W 50 ug/L <br /> stated;ND means not detected above <br /> the reporting limit S 1.0 mg/kg <br /> *water and vapor samples are reported in ug/L,wipe samples in ug/wipe,soil and sludge samples in mg/kg,and all TCLP/STLC/SPLP <br /> extracts in ug/L <br /> "cluttered chromatogram resulting in coelutcd surrogate and sample peaks,or;surrogate peak is on elevated baseline,or;surrogate has been <br /> diminished by dilution of original extract. <br /> 'The following descriptions of the TPH chromatogram are cursory in nature and McCampbell Analytical is not responsible for their <br /> interpretation:a)unmodified or weakly modified diesel is significant;b)diesel range compounds are significant;no recognizable pattern;c) <br /> C aged diesel?is significant);d)gasoline range compounds are significant;e)medium boiling point pattern that does not match diesel(?);f) <br /> one to a few isolated peaks present;g)oil range compounds are significant; h)lighter than water immiscible sheen is present; i) liquid <br /> sample that contains greater than—5 vol.%sediment, <br /> DHS Certification No. 1644 L Edward Hamilton,Lab Director <br />