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110 2nd Avenue South,##D7,Pacheco,CA 94553-5560 <br /> MCCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax: 925-798-1622 <br /> http://www.mccaMpbell,com E-mail:main@mccampbell.com <br /> John P, Cummings&Associates Client Project ID: ##0399002.00;Jamar Date Sampled: 09/08/99 <br /> P.O.Box 2847 SS Date Received: 09/13/99 <br /> Fremont, CA 94536-2847 Client Contact: John Cummings Date Extracted:09/13/99 <br /> Client P.O: Date Analyzed:09/15-09/16/99 <br /> Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br /> Lab ID 19091 1 19092 19093 19094 <br /> Reporting Limit <br /> Client ID B1-35 B1-40 B1-45 BI-50 <br /> Matrix S S S S S W <br /> Compound Concentration* ug/kg ug/L <br /> Di-isopropyl Ether(D1PE) ND<250 ND<100 ND<500 ND<1000 5.0 1.0 <br /> Ethyl tert-Butyl Ether(ETRE) ND<250 ND<100 ND<500 ND<1000 5.0 1.0 <br /> Methyl-tert Butyl Ether(MTBE) 12,000 2700 16,000 25,000 5.0 1.0 <br /> tert-Amyl Methyl Ether(TAME) ND<250 ND<100 ND<500ND<1000 5.0 1.0 <br /> tert-Butanol ND<1300 ND<500 ND<25001 ND<5000 25 5.0 <br /> Surrogate Recoveries(%) <br /> Dibromofluoromethane 101 102 102 100 <br /> Comments: <br /> •water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit;N/A means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present;(i)liquid sample that contains greater than--5 vol.%sediment;0)sample diluted due to <br /> high organic content <br /> DHS Certification No. 1644 ' . Edward Hamilton,Lab Director <br /> r . <br />