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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax:925-798-1622 <br /> httn:l/www.mccampkell.com E-mail:main@rnccampbell.com <br /> John P.Cummings&Associates Client Project ID: #0399002.00;Jamar Date Sampled:09/09/99 <br /> P.O.Box 2847 SS Date Received:09/13/99 <br /> Fremont,CA 94536-2847 Client Contact: John Cummings Date Extracted: 09/13/99 <br /> Client P.O: Date Analyzed: 09/14-09/19/99 <br /> Diesel Range(C10-C23)Extractable Hydrocarbons as Diesel* <br /> EPA methods modified 8015,and 3550 or 3510;Cal ifomia RWQCB(SF Bay Region)method GCFID(3550)or GCF1D(3510) <br /> Lab ID Client 1D Matrix TPH(d)+ °/a Recovery <br /> Surrogate <br /> 19101 132-30 S ND 105 <br /> 19102 132-35 S ND 112 <br /> 19103 132-40 S ND 115 <br /> 19104 B2-45 S ND 115 <br /> 19105 B2-50 S ND I06 <br /> 19106 132-55 S ND 100 <br /> { 19107 132-60 S ND 103 <br /> 19108 132-65 S ND 108 <br /> 19109 132-70 S ND 98 <br /> 19110 132-74 S ND 97 <br /> 19111 B3-30 S ND 109 <br /> 19112 133-35 S ND 109 <br /> 19113 133-40 S ND I10 <br /> 19114 1313-45 S 1.l,b 98 <br /> Reporting Limit unless otherwise W 50 ug/L <br /> stated;ND means not detected above <br /> the reporting limit S 1.0 mg/kg <br /> *water and vapor samples are reported in ug/L,wipe samples in ug/wipe,soil and sludge samples in mg/kg,and all TCLP/STLC/SPLP <br /> extracts in ug/L <br /> "cluttered chromatogram resulting in cocluted surrogate and sample peaks,or;surrogate peak is on elevated baseline,or;surrogate has been <br /> diminished by dilution of original extract. <br /> 'The following descriptions of the TPH chromatogram are cursory in nature and McCampbell Analytical is not responsible for their <br /> interpretation:a)unmodified or weakly modified diesel is significant;b)diesel range compounds are significant;no recognizable pattern;c) <br /> aged diesel?is significant);d)gasoline range compounds are significant;e)medium boiling point pattern that does not match diesel(?);f) <br /> one to a few isolated peaks present;g)oil range compounds are significant; h)lighter than water immiscible sheen is present; i) liquid <br /> sample that contains greater than—5 vol.%sediment. <br /> DHS Certification No. 1644 —,� Edward Hamilton,Lab Director <br />