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404 N Wlget Lane <br /> Sequoia <br /> Walnut Creek. 988-9600 <br /> FAX(975)98$-9673 <br /> Analytical10*w-%"Uowwx corn <br /> Ryan,Inc -Dublin Project Unocal <br /> 47 Slime Court suite t Project Number' Unocal#5886 Reported <br /> Dublin CA,94568 Project Manager Deanna L Harding 29-Dec-00 08 59 <br /> Volatile Organic Compounds by EPA Method 8260B- Quality Control <br /> Sequoia Analytical-Walnut Creek <br /> Reporting Spike Source QKREC RPD <br /> yte Result Lunt Units Level Result °YaREC Lantra RPD Lrrrut Notes <br /> ch OK30024-EPA 5030B[PITS <br /> Ga(OK30024-BL:K2) Prepared&Analyzed.O1-Dec-0O <br /> Ed mol ND 500 wA <br /> Butyl alcohol ND 50 " <br /> yl Ud .Ayl ether ND 20 " <br /> Dmscprnpyl ether ND 20 " <br /> iool4m4l ether ND 20 " <br /> Amyl methyl ether ND 20 " <br /> S--gaze Drbromgfluoromahaw 520 Sao 104 50.150 <br /> are 1,1 Dlchloroedwm-d4 470 SO 0 940 50450 <br /> (0100024-BIM) Prepared&Analyzes.04-Dec-00 <br /> Ethanol ND 500 US4 <br /> i alcohol ND 50 <br /> A -butyl ether ND 20 " <br /> Di-eaopeopyl ether ND 20 " <br /> tartL meth4n tyl ether ND 20 <br /> Amy yl ether ND 20 " <br /> _...'..-- <br /> S—vgate Dlbromofheoromethww S20 " Soo 104 50-150 <br /> S I,Z Dtchloroedmne-M 46.0 Sao 910 50-150 <br /> (0 0024-BS1) Prepared&Analyze&30-Nov-o0 <br /> Methyl telt-butyl ether 452 20 ugA Soo 904 70.130 <br /> au DebrvmgUoromerlrmw 490 Sao 98.0 50-150 <br /> ata 1,1 Dtchlar»edxwe-d* 440 SRO 88.0 50.150 <br /> LCS(OI M4-=) Prepared&Analyzed.01Dec-M <br /> yl tat-butyl ether 493 20 ugll Soo 98.6 70-130 <br /> ngatr Drbromofluommerlme S20 - Sao 104 50-150 <br /> Surrogate 1,1 Dichioroorhmre-d4 470 " Sao 940 50-150 <br /> S Analytical-WahW Qt& 77w remdU in rhls repmi apply ro the smnples mralyua lie acca*wce wide rhe cha n of <br /> CK"04 daemnerd This mialytical r eport naw be nprndw:ed in is nor eW <br /> ' Page 28 of 30 <br />