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1455 McDwAdl Dhd 'North Ste D <br /> Se{il oia Poaluma CA 94954 <br /> AAnalytical <br /> mir�,} (707)792 t8M5 <br /> ical IAX(70717920342 <br /> �stisc seguordabs com <br /> I RI ProItct TOSCO/11HILLIPS <br /> igital Dr Stnte 100 Project Number 58861 Stockton,Ca Repoi ted <br /> vato CA,94949 Pra)t.ct Manager Glenn Matteucci 02/08/02 16 59 <br /> Total Petroleum Hydrocarbons as Gasoline and BTEX by EPA 8015MIS020M- Quality Control <br /> Sequoia Analytical -Petaluma <br /> Reporting Spike SOtltLC %REC RPD <br /> Analyte Result Limit Units Leger Result %REC Limits RPD Lnnit Nott,- <br /> Batch 20I0570- EPA 5030,sails <br /> Blank(2010570-BLK1) Prepared&Analyzed 01/29/02 <br /> Gasoline(C6-C12) ND 1 0 mg/kg <br /> Benzene ND 00050 <br /> Toluene ND 00050 " <br /> Ethylbenzene ND 00050 " <br /> Xylenes(total) ND 00050 " <br /> Methyl tert-butyl ether ND 00050 " <br /> ,Srurogale a u a-Difluorotoluenc 0 625 0 600 104 65-135 <br /> Srorogale 4-8romofluorohenzene 0 546 0 600 91 65-135 <br /> LCS(2010570-1351) Prepared&Analyzed 01/29/02 <br /> Gasoline(C6-C 12) 515 10 mg/kg 550 94 65-135 <br /> Benzene 00914 00050 00680 134 65-135 <br /> e 0 473 00050 0 413 ]is 65-135 <br /> enzene 0 101 00050 0 0970 104 65-135 <br /> Xylenes(total) 0 509 00050 0 489 104 65-135 <br /> Methyl tert-butyl ether 0 125 00050 0 109 115 65-135 <br /> Surrogate a a a-Trifluorololuene 0 702 0 600 117 65-135 <br /> Suiragate 4-Bronrofluorohenzene 0 548 0 600 98 65-135 <br /> Matrix Spike(2010570-MS1) Source P201403-53 Prepared&Analyzed 01/29/02 <br /> Gasoline(C6-C 12) 484 1 0 mg/kg 550 ND 88 65-135 <br /> Benzene 00970 00030 00680 ND 143 65-135 QM-07 <br /> Toluene 0 502 00050 0 413 ND 121 65-135 <br /> Ethylbenzene 0 107 00050 00970 ND 110 65-135 <br /> Xylenes(total) 0 529 00050 0 489 ND 108 65-135 <br /> Methyl tert-butyl ether 0 133 00050 0 109 ND 122 65-135 <br /> Surrogate act a-Difluorololuetre 0 7?6 0 600 123 65-135 <br /> Sturogate 4-Bromofluorobenzene 0 538 0 600 90 65-135 <br /> Sola Analytical- Petaluma The results in this reportapplyto thesanrples analjzcdin accoidamt,wah the Chain of <br /> c ristods-docum(.ni This anal)ural report must he repoduced ur its entuen, <br /> Page 5 of 9 <br />