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Analytical Data <br /> Client SECOR International, Inc. Job Number: 720-7408-1 <br /> Client Sample ID: B-9 @ 50' <br /> Lab Sample ID. 720-7408-2 Date Sampled: 01/17/2007 1230 <br /> Client Matrix: Solid Date Received: 01/23/2007 0945 <br /> 8260B Volatile Organic Compounds by GC/MS <br /> Method: 8260B Analysis Batch: 720-17673 Instrument ID Saturn 2100 <br /> Preparation: 5030B Lab File ID: c:lsaturnws\data\200701\01 <br /> Dilution: 1.0 Initial Weight/Volume: 5.01 g <br /> Date Analyzed: 01/25/2007 2249 Final Weight/Volume: 10 mL <br /> Date Prepared: 01/25/2007 2249 <br /> Analyte DryWt Corrected: N Result(mg/Kg) Qualifier RL <br /> 1,2-Dichloroethane ND 0.0050 <br /> Benzene ND 0.0050 <br /> Ethanol ND <br /> 1.2 <br /> Ethylbenzene ND 0.0050 <br /> MTBE ND <br /> 0.0050 <br /> TAME ND 0.0050 <br /> Toluene ND 0.0050 <br /> Xylenes,Total ND 0.010 <br /> TBA ND <br /> 0.010 <br /> DIPE ND <br /> 0.0050 <br /> EDB <br /> ND 0.0050 <br /> Gasoline Range Organics(GRO)-C6-C12 ND 0.25 <br /> Ethyl tert-butyl ether ND 0.0050 <br /> Surrogate %Rec Acceptance Limits <br /> Toluene-d8(Surr) 93 70-130 <br /> 1,2-Dichloroethane-d4(Surr) 66 60-140 <br /> STL San Francisco Page 7 of 63 <br />