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Analytical Data <br /> Client: SECOR International, Inc. Job Number: 720-7408-1 <br /> Client Sample ID: B-7 @ 20' <br /> Lab Sample ID: 720-7408-7 Date Sampled: 01/19/2007 0925 <br /> Client Matrix: Solid Date Received: 01/23/2007 0945 <br /> 8260B Volatile Organic Compounds by GC/MS <br /> Method: 82608 Analysis Batch: 720-17644 Instrument ID: Varian 3900E <br /> Preparation: 5030B Prep Batch: 720-17645 Lab File ID: c:\varianws\data\200701\01 <br /> Dilution: 5000 Initial Weight/Volume: 5.12 g <br /> Date Analyzed: 01/26/2007 1612 Final Weight/Volume: 10 mL <br /> Date Prepared: 01/26/2007 1553 <br /> Analyte DryWt Corrected:N Result(mg/Kg) Qualifier RL <br /> 1,2-Dichloroethane ND 24 <br /> Benzene 25 24 <br /> Ethanol ND 6100 <br /> Ethylbenzene 150 24 <br /> 24 <br /> MTBE ND <br /> 24 <br /> TAME <br /> ND 24 <br /> Toluene 510 <br /> 24 <br /> Xylenes,Total 710 49 <br /> TBA ND 49 <br /> DIPE ND <br /> 24 <br /> EDB ND 24 <br /> Gasoline Range Organics(GRO)-C6-C12 8800 1200 <br /> Ethyl tert-butyl ether ND 24 <br /> Surrogate %Rec Acceptance Limits <br /> - - - - —._ <br /> Toluene-d8(Burr) 160 — X 50- 130 <br /> 1,2-Dichloroethane-d4(Surr) 115 60- 140 <br /> STL San Francisco Page 12 of 63 <br />